6-O-acetyl-2-azido-3-O-benzyl-2,4-dideoxy-D-xylo-hexopyranosyl fluoride

Base Information

Chemical Name:6-O-acetyl-2-azido-3-O-benzyl-2,4-dideoxy-D-xylo-hexopyranosyl fluoride
CAS No.:324739-93-7
Molecular Formula:C₁₅H₁₈FN₃O₄
Molecular Weight:323.324
Hs Code.:

Synonyms:6-O-acetyl-2-azido-3-O-benzyl-2,4-dideoxy-D-xylo-hexopyranosyl fluoride

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Chemical Property of 6-O-acetyl-2-azido-3-O-benzyl-2,4-dideoxy-D-xylo-hexopyranosyl fluoride

Chemical Property:

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Technology Process of 6-O-acetyl-2-azido-3-O-benzyl-2,4-dideoxy-D-xylo-hexopyranosyl fluoride

There total 4 articles about 6-O-acetyl-2-azido-3-O-benzyl-2,4-dideoxy-D-xylo-hexopyranosyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6-O-acetyl-2-azido-3-O-benzyl-2,4-dideoxy-D-xylo-hexopyranose

: 324739-93-7
6-O-acetyl-2-azido-3-O-benzyl-2,4-dideoxy-D-xylo-hexopyranosyl fluoride

Guidance literature:: With 4,4'-diaminostilbene-2,2'-disulfonic acid; In 1,2-dichloro-ethane;
DOI:10.1016/S0040-4039(00)01900-6

Reference yield:

: 55682-57-0
1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose

: 324739-93-7
6-O-acetyl-2-azido-3-O-benzyl-2,4-dideoxy-D-xylo-hexopyranosyl fluoride

Guidance literature:: Multi-step reaction with 5 steps

1: 79 percent / toluene / 2.5 h / Heating

2: 55 percent / Bu₃SnH; AIBN / benzene / 0.5 h / Heating

3: 74 percent / TFA / 20 °C

4: 81 percent / Me₂NH / acetonitrile; tetrahydrofuran / 6 h / 20 °C

5: DAST / 1,2-dichloro-ethane / -30 °C

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; dimethyl amine; 4,4'-diaminostilbene-2,2'-disulfonic acid; trifluoroacetic acid; In tetrahydrofuran; 1,2-dichloro-ethane; toluene; acetonitrile; benzene;
DOI:10.1016/j.carres.2004.02.026

Reference yield:

: 326495-54-9
1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-4-O-(thio-carbonylimidazol-1-yl)-β-D-glucopyranose

: 324739-93-7
6-O-acetyl-2-azido-3-O-benzyl-2,4-dideoxy-D-xylo-hexopyranosyl fluoride

Guidance literature:: Multi-step reaction with 4 steps

1: 55 percent / Bu₃SnH; AIBN / benzene / 0.5 h / Heating

2: 74 percent / TFA / 20 °C

3: 81 percent / Me₂NH / acetonitrile; tetrahydrofuran / 6 h / 20 °C

4: DAST / 1,2-dichloro-ethane / -30 °C

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; dimethyl amine; 4,4'-diaminostilbene-2,2'-disulfonic acid; trifluoroacetic acid; In tetrahydrofuran; 1,2-dichloro-ethane; acetonitrile; benzene;
DOI:10.1016/j.carres.2004.02.026