(2S,3S)-3-(3-Acetoxy-2-methyl-benzoylamino)-2-hydroxy-4-phenyl-butyric acid

Base Information

Chemical Name:(2S,3S)-3-(3-Acetoxy-2-methyl-benzoylamino)-2-hydroxy-4-phenyl-butyric acid
CAS No.:478411-22-2
Molecular Formula:C₂₀H₂₁NO₆
Molecular Weight:371.39
Hs Code.:

Synonyms:(2S,3S)-3-(3-Acetoxy-2-methyl-benzoylamino)-2-hydroxy-4-phenyl-butyric acid

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Chemical Property of (2S,3S)-3-(3-Acetoxy-2-methyl-benzoylamino)-2-hydroxy-4-phenyl-butyric acid

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Technology Process of (2S,3S)-3-(3-Acetoxy-2-methyl-benzoylamino)-2-hydroxy-4-phenyl-butyric acid

There total 3 articles about (2S,3S)-3-(3-Acetoxy-2-methyl-benzoylamino)-2-hydroxy-4-phenyl-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.6%

: 167678-46-8
3-acetoxy-2-methylbenzoyl chloride

: (2S,3S)-3-amino-2-hydroxy-4-phenylbutanoic acid hydrochloride

: 478411-22-2
(2S,3S)-3-(3-Acetoxy-2-methyl-benzoylamino)-2-hydroxy-4-phenyl-butyric acid

Guidance literature:: (2S,3S)-3-amino-2-hydroxy-4-phenylbutanoic acid hydrochloride; With triethylamine; In tetrahydrofuran; water;

3-acetoxy-2-methylbenzoyl chloride; In tetrahydrofuran; water; at 4 - 20 ℃; for 1h;

With hydrogenchloride; water; In tetrahydrofuran; at 10 ℃; pH=2.0; Product distribution / selectivity;

Reference yield: 92.0%

: 62023-62-5
allophenylnorstatine

: 167678-46-8
3-acetoxy-2-methylbenzoyl chloride

: 478411-22-2
(2S,3S)-3-(3-Acetoxy-2-methyl-benzoylamino)-2-hydroxy-4-phenyl-butyric acid

Guidance literature:: allophenylnorstatine; With triethylamine; In tetrahydrofuran; water; for 0.75h;

3-acetoxy-2-methylbenzoyl chloride; In tetrahydrofuran; water; at 6 ℃; for 0.5h;

With hydrogenchloride; In tetrahydrofuran; water; pH=2.5 - 8.7;