(2S,3S)-2-Acetoxy-3-(3-acetoxy-2-methyl-benzoylamino)-4-phenyl-butyric acid

Base Information

Chemical Name:(2S,3S)-2-Acetoxy-3-(3-acetoxy-2-methyl-benzoylamino)-4-phenyl-butyric acid
CAS No.:749905-01-9
Molecular Formula:C₂₂H₂₃NO₇
Molecular Weight:413.427
Hs Code.:

Synonyms:(2S,3S)-2-Acetoxy-3-(3-acetoxy-2-methyl-benzoylamino)-4-phenyl-butyric acid

Suppliers and Price of (2S,3S)-2-Acetoxy-3-(3-acetoxy-2-methyl-benzoylamino)-4-phenyl-butyric acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-2-Acetoxy-3-(3-acetoxy-2-methyl-benzoylamino)-4-phenyl-butyric acid

Chemical Property:

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Technology Process of (2S,3S)-2-Acetoxy-3-(3-acetoxy-2-methyl-benzoylamino)-4-phenyl-butyric acid

There total 2 articles about (2S,3S)-2-Acetoxy-3-(3-acetoxy-2-methyl-benzoylamino)-4-phenyl-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.5%

: 478411-22-2
(2S,3S)-3-(3-Acetoxy-2-methyl-benzoylamino)-2-hydroxy-4-phenyl-butyric acid

: 108-24-7
acetic anhydride

: 749905-01-9
(2S,3S)-2-Acetoxy-3-(3-acetoxy-2-methyl-benzoylamino)-4-phenyl-butyric acid

Guidance literature:: With methanesulfonic acid; In ethyl acetate; at 25 - 70 ℃; for 3h;

Reference yield: 74.5%

: 108-24-7
acetic anhydride

: 62023-62-5
allophenylnorstatine

: 167678-46-8
3-acetoxy-2-methylbenzoyl chloride

: 749905-01-9
(2S,3S)-2-Acetoxy-3-(3-acetoxy-2-methyl-benzoylamino)-4-phenyl-butyric acid

Guidance literature:: allophenylnorstatine; With triethylamine; sodium chloride; In tetrahydrofuran; water; at 20 ℃;

3-acetoxy-2-methylbenzoyl chloride; In tetrahydrofuran; water; at 5 - 10 ℃; for 1h;

acetic anhydride; With hydrogenchloride; methanesulfonic acid; more than 3 stages;

Reference yield:

: 749905-01-9
(2S,3S)-2-Acetoxy-3-(3-acetoxy-2-methyl-benzoylamino)-4-phenyl-butyric acid

: 749905-00-8
(R)-5,5-Dimethyl-thiazolidine-4-carboxylic acid allylamide hydrochloride

: 853411-65-1
acetic acid 3-{(1S,2S)-2-acetoxy-3-[(4R)-4-allylcarbamoyl-5,5-dimethyl-thiazolidin-3-yl]-1-benzyl-3-oxo-propylcarbamoyl}-2-methyl-phenyl ester

Guidance literature:: (2S,3S)-2-Acetoxy-3-(3-acetoxy-2-methyl-benzoylamino)-4-phenyl-butyric acid; With pyridine; thionyl chloride; In acetonitrile; at 15 ℃; for 1h;

(R)-5,5-Dimethyl-thiazolidine-4-carboxylic acid allylamide hydrochloride; In acetonitrile; at 15 ℃; for 6h;