4-((4-((2-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N,N-diethylbenzamidine

Base Information

Chemical Name:4-((4-((2-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N,N-diethylbenzamidine
CAS No.:1634648-94-4
Molecular Formula:C₂₁H₂₄N₆O₃
Molecular Weight:408.46
Hs Code.:

Synonyms:4-((4-((2-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N,N-diethylbenzamidine

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Chemical Property of 4-((4-((2-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N,N-diethylbenzamidine

Chemical Property:

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Technology Process of 4-((4-((2-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N,N-diethylbenzamidine

There total 7 articles about 4-((4-((2-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N,N-diethylbenzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₁₉N₅O₄

: 109-89-7
diethylamine

: 1634648-94-4
4-((4-((2-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N,N-diethylbenzamidine

Guidance literature:: In methanol; for 24h;
DOI:10.3390/molecules19055674

Reference yield:

: 1634648-91-1
4-((4-((2-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)benzonitrile

: 1634648-94-4
4-((4-((2-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N,N-diethylbenzamidine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 48 h / 20 °C / Cooling with ice

2: methanol / 24 h

With hydrogenchloride; In methanol; 1: |Pinner Amidine Synthesis;
DOI:10.3390/molecules19055674

Reference yield:

: 13350-09-9
1-nitro-2-(prop-2-yn-1-yloxy)benzene

: 1634648-94-4
4-((4-((2-nitrophenoxy)methyl)-1H-1,2,3-triazol-1-yl)methyl)-N,N-diethylbenzamidine

Guidance literature:: Multi-step reaction with 3 steps

1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 24 h / 60 °C

2: hydrogenchloride / 48 h / 20 °C / Cooling with ice

3: methanol / 24 h

With hydrogenchloride; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In methanol; water; tert-butyl alcohol; 2: |Pinner Amidine Synthesis;
DOI:10.3390/molecules19055674