(S)-4-(3-diazo-3-(diethoxyphosphoryl)-2-(1,3-dioxoisoindolin-2-yl)propyl)phenyl acetate

Base Information

Chemical Name:(S)-4-(3-diazo-3-(diethoxyphosphoryl)-2-(1,3-dioxoisoindolin-2-yl)propyl)phenyl acetate
CAS No.:1583285-46-4
Molecular Formula:C₂₃H₂₄N₃O₇P
Molecular Weight:485.433
Hs Code.:

Synonyms:(S)-4-(3-diazo-3-(diethoxyphosphoryl)-2-(1,3-dioxoisoindolin-2-yl)propyl)phenyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-4-(3-diazo-3-(diethoxyphosphoryl)-2-(1,3-dioxoisoindolin-2-yl)propyl)phenyl acetate

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Technology Process of (S)-4-(3-diazo-3-(diethoxyphosphoryl)-2-(1,3-dioxoisoindolin-2-yl)propyl)phenyl acetate

There total 6 articles about (S)-4-(3-diazo-3-(diethoxyphosphoryl)-2-(1,3-dioxoisoindolin-2-yl)propyl)phenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: C₃₀H₃₂N₃O₉PS

: 1583285-46-4
(S)-4-(3-diazo-3-(diethoxyphosphoryl)-2-(1,3-dioxoisoindolin-2-yl)propyl)phenyl acetate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; Schlenk technique;
DOI:10.1002/adsc.201300838

Reference yield:

: 65594-96-9
O-Acetyl-N-phthaloyltyrosin

: 1583285-46-4
(S)-4-(3-diazo-3-(diethoxyphosphoryl)-2-(1,3-dioxoisoindolin-2-yl)propyl)phenyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / toluene / Reflux; Schlenk technique

2: dichloromethane / 20 °C / Schlenk technique

3: hydrogenchloride / tetrahydrofuran / 20 °C / Schlenk technique

4: triethylamine / dichloromethane / 20 °C / Schlenk technique

With hydrogenchloride; thionyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; toluene; 2: |Arbuzov Reaction;
DOI:10.1002/adsc.201300838

Reference yield:

: 85-44-9
phthalic anhydride

: 1583285-46-4
(S)-4-(3-diazo-3-(diethoxyphosphoryl)-2-(1,3-dioxoisoindolin-2-yl)propyl)phenyl acetate

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid / Reflux; Schlenk technique

2: thionyl chloride / toluene / Reflux; Schlenk technique

3: dichloromethane / 20 °C / Schlenk technique

4: hydrogenchloride / tetrahydrofuran / 20 °C / Schlenk technique

5: triethylamine / dichloromethane / 20 °C / Schlenk technique

With hydrogenchloride; thionyl chloride; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane; toluene; 3: |Arbuzov Reaction;
DOI:10.1002/adsc.201300838