3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methoxy-(1S)-methyl-ethoxy)-benzoic acid

Base Information

Chemical Name:3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methoxy-(1S)-methyl-ethoxy)-benzoic acid
CAS No.:1282521-11-2
Molecular Formula:C₁₆H₂₅O₇P
Molecular Weight:360.344
Hs Code.:

Synonyms:3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methoxy-(1S)-methyl-ethoxy)-benzoic acid

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Chemical Property of 3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methoxy-(1S)-methyl-ethoxy)-benzoic acid

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Technology Process of 3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methoxy-(1S)-methyl-ethoxy)-benzoic acid

There total 4 articles about 3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methoxy-(1S)-methyl-ethoxy)-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.6%

: 1282521-09-8
3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methoxy-(1S)-methyl-ethoxy)-benzoic acid methyl ester

: 1282521-11-2
3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methoxy-(1S)-methyl-ethoxy)-benzoic acid

Guidance literature:: 3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methoxy-(1S)-methyl-ethoxy)-benzoic acid methyl ester; With sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 12h;

With hydrogenchloride; In water;

Reference yield:

: 1282520-98-2
dimethyl 5-hydroxy isophthalate

: 1282521-11-2
3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methoxy-(1S)-methyl-ethoxy)-benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: tribromo phosphate / tetrahydrofuran / 12 h / 0 - 20 °C

2: 3 h / 160 °C

3: sodium hydroxide / tetrahydrofuran / 12 h / 20 °C

With tribromo phosphate; sodium hydroxide; In tetrahydrofuran;

Reference yield:

: 1282520-90-4
5-(2-methoxy-(1S)-methyl-ethoxy)isophthalic acid monomethyl ester

: 1282521-11-2
3-[(phosphonic acid diethyl ester)-methyl]-5-(2-methoxy-(1S)-methyl-ethoxy)-benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: borane-THF / tetrahydrofuran / 12 h / 0 - 20 °C

1.2: 3 h / 0 °C

2.1: tribromo phosphate / tetrahydrofuran / 12 h / 0 - 20 °C

3.1: 3 h / 160 °C

4.1: sodium hydroxide / tetrahydrofuran / 12 h / 20 °C

With borane-THF; tribromo phosphate; sodium hydroxide; In tetrahydrofuran;