(((2-(benzyloxy)propane-1,3-diyl)bis(oxy))bis(methanetetrayl))hexabenzene

Base Information

• Chemical Name: (((2-(benzyloxy)propane-1,3-diyl)bis(oxy))bis(methanetetrayl))hexabenzene
• CAS No.: 114838-37-8
• Molecular Formula: C₄₈H₄₂O₃
• Molecular Weight: 666.86

Synonyms:(((2-(benzyloxy)propane-1,3-diyl)bis(oxy))bis(methanetetrayl))hexabenzene

Chemical Property of (((2-(benzyloxy)propane-1,3-diyl)bis(oxy))bis(methanetetrayl))hexabenzene

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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MSDS Files:

SDS file from LookChem

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Technology Process of (((2-(benzyloxy)propane-1,3-diyl)bis(oxy))bis(methanetetrayl))hexabenzene

There total 6 articles about (((2-(benzyloxy)propane-1,3-diyl)bis(oxy))bis(methanetetrayl))hexabenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

benzyl bromide (100-39-0) + trityl chloride (76-83-5) + glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) → 1,2,3-tri-O-tritylglycerol + (((2-(benzyloxy)propane-1,3-diyl)bis(oxy))bis(methanetetrayl))hexabenzene (114838-37-8)

Guidance literature:

trityl chloride; glycerol; With pyridine; at 20 ℃; for 24h;

benzyl bromide; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; Further stages.;

DOI:10.1016/j.tet.2008.08.010

Reference yield: 70.0%

trityl chloride (76-83-5) + benzyl chloride (100-44-7) + glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) → 1,2,3-tri-O-tritylglycerol + (((2-(benzyloxy)propane-1,3-diyl)bis(oxy))bis(methanetetrayl))hexabenzene (114838-37-8)

Guidance literature:

trityl chloride; glycerol; With pyridine; at 100 ℃; for 1h;

benzyl chloride; With potassium hydroxide; In toluene; for 1h; Further stages.; Heating;

DOI:10.1016/j.tet.2008.08.010

Reference yield:

1,3-bis (trityloxy)propan-2-ol (5443-10-7) + benzyl bromide (100-39-0) → (((2-(benzyloxy)propane-1,3-diyl)bis(oxy))bis(methanetetrayl))hexabenzene (114838-37-8)

Guidance literature:

With sodium hydride; In tetrahydrofuran; Yield given;

DOI:10.1021/jo00248a046

upstream raw materials:

1,3-bis (trityloxy)propan-2-ol

benzyl bromide

benzyl chloride

trityl chloride

Downstream raw materials:

2-O-benzylglycerol

1-O-acetyl-2-O-benzyl-(R,S)-glycerol

(S)-2-(benzyloxy)-3-hydroxypropyl acetate

2-O-benzyl-1-O-(2,3,6,2',3',4',6'-hepta-O-acetyl-β-lactosyl)-(R,S)-glycerol

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