3-Benzyloxybenzaldehyde dimethyl acetal

Base Information

• Chemical Name: 3-Benzyloxybenzaldehyde dimethyl acetal
• CAS No.: 298704-00-4
• Molecular Formula: C₁₆H₁₈O₃
• Molecular Weight: 258.317
• Mol file: 298704-00-4.mol

Synonyms:3-Benzyloxybenzaldehyde dimethyl acetal

Chemical Property of 3-Benzyloxybenzaldehyde dimethyl acetal

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 3-Benzyloxybenzaldehyde dimethyl acetal

There total 1 articles about 3-Benzyloxybenzaldehyde dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

3-Benzyloxybenzaldehyde (1700-37-4) + 2,2-dimethoxy-propane (77-76-9) → 3-Benzyloxybenzaldehyde dimethyl acetal (298704-00-4)

Guidance literature:

With toluene-4-sulfonic acid; at 70 ℃;

DOI:10.1039/b002101f

Reference yield: 82.0%

(S)-3-acetyl-4-isopropyl-1,3-thiazolidine-2-thione (101979-45-7) + 3-Benzyloxybenzaldehyde dimethyl acetal (298704-00-4) → (S)-3-(3-Benzyloxy-phenyl)-1-((S)-4-isopropyl-2-thioxo-thiazolidin-3-yl)-3-methoxy-propan-1-one (909391-19-1)

Guidance literature:

(S)-3-acetyl-4-isopropyl-1,3-thiazolidine-2-thione; With titanium tetrachloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 ℃; for 2h;

3-Benzyloxybenzaldehyde dimethyl acetal; With boron trifluoride diethyl etherate; In dichloromethane; for 2h;

DOI:10.1016/j.tetlet.2006.05.187

Reference yield: 68.0%

3-Benzyloxybenzaldehyde dimethyl acetal (298704-00-4) + phosphorous acid trimethyl ester (121-45-9) → Dimethyl 1-methoxy-1-(3-benzyloxyphenyl)methylphosphonate

Guidance literature:

With chloro-trimethyl-silane; at 20 ℃; for 80h;

DOI:10.1039/b002101f

upstream raw materials:

3-Benzyloxybenzaldehyde

2,2-dimethoxy-propane

Downstream raw materials:

(S)-3-(3-Benzyloxy-phenyl)-1-((S)-4-isopropyl-2-thioxo-thiazolidin-3-yl)-3-methoxy-propan-1-one

1-Benzyloxy-3-((S)-3-iodo-1-methoxy-propyl)-benzene

(S)-3-(3-Benzyloxy-phenyl)-3-methoxy-propan-1-ol

(2S,5S)-5-(3-Benzyloxy-phenyl)-5-methoxy-2-methyl-pentanal