methyl 6-(tert-butyldimethylsilyloxy)-3-O-(benzoyl)-β-D-galactopyranoside

Base Information

Chemical Name:methyl 6-(tert-butyldimethylsilyloxy)-3-O-(benzoyl)-β-D-galactopyranoside
CAS No.:1610558-83-2
Molecular Formula:C₂₀H₃₂O₇Si
Molecular Weight:412.555
Hs Code.:

Synonyms:methyl 6-(tert-butyldimethylsilyloxy)-3-O-(benzoyl)-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 6-(tert-butyldimethylsilyloxy)-3-O-(benzoyl)-β-D-galactopyranoside

Chemical Property:

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Technology Process of methyl 6-(tert-butyldimethylsilyloxy)-3-O-(benzoyl)-β-D-galactopyranoside

There total 5 articles about methyl 6-(tert-butyldimethylsilyloxy)-3-O-(benzoyl)-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 74247-82-8,63734-12-3,74247-81-7,74264-88-3
Methyl 6-O-<(1,1-dimethylethyl)dimethylsilyl>-β-D-galactopyranoside

: 93-97-0
benzoic acid anhydride

: 1610558-83-2
methyl 6-(tert-butyldimethylsilyloxy)-3-O-(benzoyl)-β-D-galactopyranoside

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 40 ℃; regioselective reaction; Green chemistry;
DOI:10.1039/c8ob01464g

Reference yield: 95.0%

: 74247-82-8,63734-12-3,74247-81-7,74264-88-3
Methyl 6-O-<(1,1-dimethylethyl)dimethylsilyl>-β-D-galactopyranoside

: 98-88-4
benzoyl chloride

: 1610558-83-2
methyl 6-(tert-butyldimethylsilyloxy)-3-O-(benzoyl)-β-D-galactopyranoside

Guidance literature:: With sodium bromide; silver(l) oxide; In acetonitrile; at 20 ℃; for 24h; regioselective reaction;
DOI:10.1002/cctc.201601558

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1610558-83-2
methyl 6-(tert-butyldimethylsilyloxy)-3-O-(benzoyl)-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; N,N-dimethyl-formamide / acetonitrile / 0.5 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / acetonitrile / 10 h / 40 °C

With triethylamine; N-ethyl-N,N-diisopropylamine; N,N-dimethyl-formamide; In acetonitrile;
DOI:10.1002/ejoc.201901195