4,4'-Diphenyl-4H,4'H-[2,2']bi[[1,3,4]thiadiazolyl]-5,5'-diylidenediamine

Base Information

• Chemical Name: 4,4'-Diphenyl-4H,4'H-[2,2']bi[[1,3,4]thiadiazolyl]-5,5'-diylidenediamine
• CAS No.: 155959-86-7
• Molecular Formula: C₁₆H₁₂N₆S₂
• Molecular Weight: 352.443
• Mol file: 155959-86-7.mol

Synonyms:4,4'-Diphenyl-4H,4'H-[2,2']bi[[1,3,4]thiadiazolyl]-5,5'-diylidenediamine

Chemical Property of 4,4'-Diphenyl-4H,4'H-[2,2']bi[[1,3,4]thiadiazolyl]-5,5'-diylidenediamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,4'-Diphenyl-4H,4'H-[2,2']bi[[1,3,4]thiadiazolyl]-5,5'-diylidenediamine

There total 2 articles about 4,4'-Diphenyl-4H,4'H-[2,2']bi[[1,3,4]thiadiazolyl]-5,5'-diylidenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

N,N'-diphenylethane(bis-hydrazonoyl dichloride) (31805-14-8) + potassium thioacyanate (333-20-0) → 4,4'-Diphenyl-4H,4'H-[2,2']bi[[1,3,4]thiadiazolyl]-5,5'-diylidenediamine (155959-86-7)

Guidance literature:

In ethanol; water; for 3h; Product distribution; Heating; reactions of derivatives with var. reagents;

DOI:10.1016/S0040-4020(01)90419-3

Reference yield:

N,N'-diphenylethane(bis-hydrazonoyl dichloride) (31805-14-8) + thiourea (17356-08-0) → 4,4'-Diphenyl-4H,4'H-[2,2']bi[[1,3,4]thiadiazolyl]-5,5'-diylidenediamine (155959-86-7)

Guidance literature:

In ethanol; for 3h; Heating;

DOI:10.1016/S0040-4020(01)90419-3

Reference yield: 87.0%

benzoyl chloride (98-88-4) + 4,4'-Diphenyl-4H,4'H-[2,2']bi[[1,3,4]thiadiazolyl]-5,5'-diylidenediamine (155959-86-7) → C30H20N6O2S2

Guidance literature:

With pyridine; for 0.5h; Heating;

DOI:10.1016/S0040-4020(01)90419-3

upstream raw materials:

N,N'-diphenylethane(bis-hydrazonoyl dichloride)

potassium thioacyanate

thiourea

Downstream raw materials:

C₁₆H₁₀N₈O₂S₂