Technology Process of C14H15NO2
There total 5 articles about C14H15NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
acetonitrile;
at 150 ℃;
for 1h;
Inert atmosphere;
Microwave irradiation;
DOI:10.1021/ol4010195
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: calcium oxide; phosphorus pentoxide / chloroform / Inert atmosphere
1.2: Inert atmosphere
2.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 4 h / -78 - 0 °C / Inert atmosphere
3.1: triethylamine / acetonitrile / 1 h / 150 °C / Inert atmosphere; Microwave irradiation
With
phosphorus pentoxide; diisobutylaluminium hydride; triethylamine; calcium oxide;
In
tetrahydrofuran; chloroform; toluene; acetonitrile;
DOI:10.1021/ol4010195
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
2.1: calcium oxide; phosphorus pentoxide / chloroform / Inert atmosphere
2.2: Inert atmosphere
3.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 4 h / -78 - 0 °C / Inert atmosphere
4.1: triethylamine / acetonitrile / 1 h / 150 °C / Inert atmosphere; Microwave irradiation
With
phosphorus pentoxide; diisobutylaluminium hydride; triethylamine; calcium oxide;
In
tetrahydrofuran; dichloromethane; chloroform; toluene; acetonitrile;
DOI:10.1021/ol4010195
