α-methyl (2S,3S)-N-trifluoroacetyl-3-methylaspartyl-m-chlorobenzoyl peroxide

Base Information

Chemical Name:α-methyl (2S,3S)-N-trifluoroacetyl-3-methylaspartyl-m-chlorobenzoyl peroxide
CAS No.:115527-73-6
Molecular Formula:C₁₅H₁₃ClF₃NO₇
Molecular Weight:411.719
Hs Code.:

Synonyms:α-methyl (2S,3S)-N-trifluoroacetyl-3-methylaspartyl-m-chlorobenzoyl peroxide

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Chemical Property of α-methyl (2S,3S)-N-trifluoroacetyl-3-methylaspartyl-m-chlorobenzoyl peroxide

Chemical Property:

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Technology Process of α-methyl (2S,3S)-N-trifluoroacetyl-3-methylaspartyl-m-chlorobenzoyl peroxide

There total 3 articles about α-methyl (2S,3S)-N-trifluoroacetyl-3-methylaspartyl-m-chlorobenzoyl peroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 115527-71-4
α-methyl N-trifluoroacetyl-(2S,3S)-3-methylaspartyl-β-acid-chloride

: 937-14-4
3-chloro-benzenecarboperoxoic acid

: 115527-73-6
α-methyl (2S,3S)-N-trifluoroacetyl-3-methylaspartyl-m-chlorobenzoyl peroxide

Guidance literature:: With pyridine; In diethyl ether; at 0 ℃; for 4h;
DOI:10.1016/S0040-4020(01)87712-7

Reference yield:

: 498-24-8,7407-59-2
Mesaconic acid

: 115527-73-6
α-methyl (2S,3S)-N-trifluoroacetyl-3-methylaspartyl-m-chlorobenzoyl peroxide

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / β-methylaspartase, Mg(2+), K(1+) / H2O / 40 h / 30 °C

3: 60 percent / pyridine / diethyl ether / 4 h / 0 °C

With pyridine; β-methylaspartase; magnesium(II); potassium ion; In diethyl ether; water;
DOI:10.1016/S0040-4020(01)87712-7

Reference yield:

: 6061-13-8
(2S,3S)-3-methylaspartic acid

: 115527-73-6
α-methyl (2S,3S)-N-trifluoroacetyl-3-methylaspartyl-m-chlorobenzoyl peroxide

Guidance literature:: Multi-step reaction with 2 steps

2: 60 percent / pyridine / diethyl ether / 4 h / 0 °C

With pyridine; In diethyl ether;
DOI:10.1016/S0040-4020(01)87712-7