3-(2-(3,4-dimethoxyphenyl)propan-2-yl)-4-(4-fluorophenyl)-1H-1,2,4-triazole-5(4H)-thione

Base Information

Chemical Name:3-(2-(3,4-dimethoxyphenyl)propan-2-yl)-4-(4-fluorophenyl)-1H-1,2,4-triazole-5(4H)-thione
CAS No.:1239964-46-5
Molecular Formula:C₁₉H₂₀FN₃O₂S
Molecular Weight:373.451
Hs Code.:

Synonyms:3-(2-(3,4-dimethoxyphenyl)propan-2-yl)-4-(4-fluorophenyl)-1H-1,2,4-triazole-5(4H)-thione

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Chemical Property of 3-(2-(3,4-dimethoxyphenyl)propan-2-yl)-4-(4-fluorophenyl)-1H-1,2,4-triazole-5(4H)-thione

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Technology Process of 3-(2-(3,4-dimethoxyphenyl)propan-2-yl)-4-(4-fluorophenyl)-1H-1,2,4-triazole-5(4H)-thione

There total 5 articles about 3-(2-(3,4-dimethoxyphenyl)propan-2-yl)-4-(4-fluorophenyl)-1H-1,2,4-triazole-5(4H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 2-(2-(3,4-dimethoxyphenyl)-2-methylpropanoyl)-N-(4-fluorophenyl)hydrazinecarbothioamide

: 1239964-46-5
3-(2-(3,4-dimethoxyphenyl)propan-2-yl)-4-(4-fluorophenyl)-1H-1,2,4-triazole-5(4H)-thione

Guidance literature:: 2-(2-(3,4-dimethoxyphenyl)-2-methylpropanoyl)-N-(4-fluorophenyl)hydrazinecarbothioamide; With sodium hydroxide; Reflux;

With hydrogenchloride; In water; at 20 ℃; pH=5;

Reference yield:

: 23023-16-7
2‐(3,4‐dimethoxyphenyl)‐2‐methylpropionitrile

: 1239964-46-5
3-(2-(3,4-dimethoxyphenyl)propan-2-yl)-4-(4-fluorophenyl)-1H-1,2,4-triazole-5(4H)-thione

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid; water / 7 h / Reflux

2.1: sulfuric acid / 12 h / Reflux

3.1: hydrazine hydrate / methanol / 18 h / 110 °C / sealed tube

4.1: ethanol / 2 h / Reflux

5.1: sodium hydroxide / Reflux

5.2: 20 °C / pH 5

With sulfuric acid; water; hydrazine hydrate; sodium hydroxide; sulfuric acid; In methanol; ethanol;

Reference yield:

: 59212-11-2
2-(3,4-dimethoxyphenyl)-2-methylpropanoic acid

: 1239964-46-5
3-(2-(3,4-dimethoxyphenyl)propan-2-yl)-4-(4-fluorophenyl)-1H-1,2,4-triazole-5(4H)-thione

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfuric acid / 12 h / Reflux

2.1: hydrazine hydrate / methanol / 18 h / 110 °C / sealed tube

3.1: ethanol / 2 h / Reflux

4.1: sodium hydroxide / Reflux

4.2: 20 °C / pH 5

With hydrazine hydrate; sodium hydroxide; sulfuric acid; In methanol; ethanol;