N-(4-bromo-2-chloro-6-(trifluoromethyl)phenyl)-3,3-dimethylbutanamide

Base Information

• Chemical Name: N-(4-bromo-2-chloro-6-(trifluoromethyl)phenyl)-3,3-dimethylbutanamide
• CAS No.: 1009344-66-4
• Molecular Formula: C₁₃H₁₄BrClF₃NO
• Molecular Weight: 372.612

Synonyms:N-(4-bromo-2-chloro-6-(trifluoromethyl)phenyl)-3,3-dimethylbutanamide

Chemical Property of N-(4-bromo-2-chloro-6-(trifluoromethyl)phenyl)-3,3-dimethylbutanamide

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Technology Process of N-(4-bromo-2-chloro-6-(trifluoromethyl)phenyl)-3,3-dimethylbutanamide

There total 1 articles about N-(4-bromo-2-chloro-6-(trifluoromethyl)phenyl)-3,3-dimethylbutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3-dimethylbutanoic acid chloride (7065-46-5) + 4-bromo-2-chloro-6-(trifluoromethyl)aniline (870703-71-2) → N-(4-bromo-2-chloro-6-(trifluoromethyl)phenyl)-3,3-dimethylbutanamide (1009344-66-4)

Guidance literature:

In acetonitrile; at 20 ℃;

Reference yield: 47.0%

1,2,3,4-tetrahydroisoquinoline (91-21-4) + N-(4-bromo-2-chloro-6-(trifluoromethyl)phenyl)-3,3-dimethylbutanamide (1009344-66-4) → N-(2-chloro-4-(3,4-dihydroisoquinolin-2(1H)-yl)-6-(trifluoromethyl)phenyl)-3,3-dimethylbutanamide (1009344-19-7)

Guidance literature:

With potassium tert-butylate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; DavePhos; In toluene; at 90 ℃;

Reference yield:

6-fluoro-1,2,3,4-tetrahydroisoquinoline (224161-37-9) + N-(4-bromo-2-chloro-6-(trifluoromethyl)phenyl)-3,3-dimethylbutanamide (1009344-66-4) → N-(2-chloro-4-(6-fluoro-3,4-dihydroisoquinolin-2(1H)-yl)-6-(trifluoromethyl)phenyl)-3,3-dimethylbutanamide (1009344-24-4)

Guidance literature:

With potassium tert-butylate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; DavePhos; In toluene; at 90 ℃;

upstream raw materials:

3,3-dimethylbutanoic acid chloride

4-bromo-2-chloro-6-(trifluoromethyl)aniline

Downstream raw materials:

N-(2-chloro-4-(3,4-dihydroisoquinolin-2(1H)-yl)-6-(trifluoromethyl)phenyl)-3,3-dimethylbutanamide

N-(2-chloro-4-(6-fluoro-3,4-dihydroisoquinolin-2(1H)-yl)-6-(trifluoromethyl)phenyl)-3,3-dimethylbutanamide

N-[2-chloro-4-(7-fluoro-3,4-dihydro-1H-isoquinolin-2-yl)-6-trifluoromethyl-phenyl]-3,3-dimethylbutanamide

N-[2-Chloro-4-(6-chloro-3,4-dihydro-1H-isoquinolin-2-yl)-6-trifluoromethyl-phenyl]-3,3-dimethyl-butanamide

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