2-(3,3-difluoro-2-phenylallyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(3,3-difluoro-2-phenylallyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1325729-51-8
Molecular Formula:C₁₅H₁₉BF₂O₂
Molecular Weight:280.122
Hs Code.:

Synonyms:2-(3,3-difluoro-2-phenylallyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(3,3-difluoro-2-phenylallyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of 2-(3,3-difluoro-2-phenylallyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 1 articles about 2-(3,3-difluoro-2-phenylallyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 384-64-5
3,3,3-trifluoro-2-phenylpropene

: 73183-34-3
bis(pinacol)diborane

: 1325729-51-8
2-(3,3-difluoro-2-phenylallyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With iron(II) chloride; lithium tert-butoxide; In tetrahydrofuran; at 65 ℃; for 2h; Solvent; Reagent/catalyst; Temperature; Catalytic behavior; Inert atmosphere; Schlenk technique;

Reference yield: 97.0%

: 1325729-51-8
2-(3,3-difluoro-2-phenylallyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1624-53-9,3230-45-3,137838-23-4
2-(benzylideneamino)phenol

: 2-((2,2-difluoro-1,3-diphenylbut-3-en-1-yl)amino)phenol

Guidance literature:: With methanol; In tetrahydrofuran; at 20 ℃; for 24h; regioselective reaction;
DOI:10.1039/c8ob00541a

Reference yield: 96.0%

: 1325729-51-8
2-(3,3-difluoro-2-phenylallyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 100-52-7
benzaldehyde

: 95-55-6
2-amino-phenol

: 2-((2,2-difluoro-1,3-diphenylbut-3-en-1-yl)amino)phenol

Guidance literature:: benzaldehyde; 2-amino-phenol; In methanol; at 20 ℃; for 2h; Molecular sieve;

2-(3,3-difluoro-2-phenylallyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In methanol; at 20 ℃; for 5h; Molecular sieve; Inert atmosphere;
DOI:10.1021/acs.orglett.8b00721