1-ethyl-4-phenoxybenzene

Base Information

• Chemical Name: 1-ethyl-4-phenoxybenzene
• CAS No.: 36207-23-5
• Molecular Formula: C₁₄H₁₄O
• Molecular Weight: 198.265
• Mol file: 36207-23-5.mol

Synonyms:1-ethyl-4-phenoxybenzene

Chemical Property of 1-ethyl-4-phenoxybenzene

Chemical Property:

• Boiling Point: 112-114 °C(Press: 2-3 Torr)
• Density: 1.037 g/cm3

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-ethyl-4-phenoxybenzene

There total 12 articles about 1-ethyl-4-phenoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

bromobenzene (108-86-1,52753-63-6) + 4-Ethylphenol (123-07-9) → 1-ethyl-4-phenoxybenzene (36207-23-5)

Guidance literature:

With caesium carbonate; at 130 ℃; for 2.5h; Inert atmosphere;

DOI:10.1039/c3cy00082f

Reference yield: 90.0%

4-Ethylphenol (123-07-9) + iodobenzene (591-50-4) → 1-ethyl-4-phenoxybenzene (36207-23-5)

Guidance literature:

With caesium carbonate; at 130 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c3cy00082f

Reference yield: 84.0%

1-(4-ethynylphenoxy)benzene (4200-06-0) → 1-ethyl-4-phenoxybenzene (36207-23-5)

Guidance literature:

With (S)-(+)-5,5’-bis[di(3,5-di-tert-butyl-4-methoxyphenyl)phosphino]-4,4’-bi-1,3-benzodioxole; (dimethoxy)methylsilane; copper diacetate; isopropyl alcohol; In tetrahydrofuran; at 60 ℃; for 9h; Sealed tube; Inert atmosphere;

DOI:10.1021/acs.orglett.0c03632

upstream raw materials:

diphenylether

chloroethane

4-phenoxystyrene

1-(4-phenoxyphenyl)ethyl alcohol

Downstream raw materials:

4-phenoxystyrene

4-phenoxyacetophenone