Butyl-[(2Z,4Z,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine

Base Information

• Chemical Name: Butyl-[(2Z,4Z,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine
• CAS No.: 52647-48-0
• Molecular Formula: C₂₄H₃₇N
• Molecular Weight: 339.564

Synonyms:Butyl-[(2Z,4Z,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine

Chemical Property of Butyl-[(2Z,4Z,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine

Chemical Property:

Purity/Quality:

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Technology Process of Butyl-[(2Z,4Z,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine

There total 12 articles about Butyl-[(2Z,4Z,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

all-trans-Retinal (116-31-4) + N-butylamine (109-73-9,85404-21-3) → trans-N-retinylidene-n-butylimine (36076-04-7,51804-54-7,51847-39-3,52647-48-0,61769-47-9,68737-92-8,68737-93-9,68737-94-0,74644-89-6,80736-10-3,92216-30-3,98462-61-4,100836-89-3,120201-10-7,34512-76-0)

Guidance literature:

With 3 A molecular sieve; In diethyl ether; at -20 ℃; for 24h;

DOI:10.1002/hlca.19810640702

Reference yield: 8.0%

13-cis-vitamin A aldehyde (472-86-6) + N-butylamine (109-73-9,85404-21-3) → butyl-(13Z,15E)-retinylidene-amine (68737-92-8) + trans-N-retinylidene-n-butylimine (36076-04-7,51804-54-7,51847-39-3,52647-48-0,61769-47-9,68737-92-8,68737-93-9,68737-94-0,74644-89-6,80736-10-3,92216-30-3,98462-61-4,100836-89-3,120201-10-7,34512-76-0) + 1-Butyl-4-methyl-2-[(1E,3E)-2-methyl-4-(2,6,6-trimethyl-cyclohex-1-enyl)-buta-1,3-dienyl]-1,2-dihydro-pyridine (115031-66-8)

Guidance literature:

With 4 A molecular sieve; In ethanol; 1) 0 deg C, 1 h; 2) rt, 1 h;

DOI:10.1021/ja00221a084

Reference yield:

11-cis,13-cis-retinal (564-88-5) + N-butylamine (109-73-9,85404-21-3) → Butyl-[(2Z,4Z,6E,8E)-3,7-dimethyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,4,6,8-tetraen-(E)-ylidene]-amine (52647-48-0)

Guidance literature:

With 3 A molecular sieve; In methanol; at 0 ℃; for 12h;

DOI:10.1021/ja00370a043

upstream raw materials:

(11Z)-retinal

N-butylamine

all-trans-Retinal

butyl-(9Z,15E)-retinylidene-amine

Downstream raw materials:

trans-retinylidene-n-butylamine

butyl-(9Z,15E)-retinylidene-amine

butyl-(13Z,15Z)-retinylidene-amine

1-Butyl-4-methyl-2-[(1E,3E)-2-methyl-4-(2,6,6-trimethyl-cyclohex-1-enyl)-buta-1,3-dienyl]-1,2-dihydro-pyridine

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