(3-(1-(ethoxycarbamoyl)ethyl)phenyl)(phenyl)methyl ethoxycarbamate

Base Information

Chemical Name:(3-(1-(ethoxycarbamoyl)ethyl)phenyl)(phenyl)methyl ethoxycarbamate
CAS No.:1218923-26-2
Molecular Formula:C₂₁H₂₆N₂O₅
Molecular Weight:386.448
Hs Code.:

Synonyms:(3-(1-(ethoxycarbamoyl)ethyl)phenyl)(phenyl)methyl ethoxycarbamate

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Chemical Property of (3-(1-(ethoxycarbamoyl)ethyl)phenyl)(phenyl)methyl ethoxycarbamate

Chemical Property:

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Technology Process of (3-(1-(ethoxycarbamoyl)ethyl)phenyl)(phenyl)methyl ethoxycarbamate

There total 3 articles about (3-(1-(ethoxycarbamoyl)ethyl)phenyl)(phenyl)methyl ethoxycarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1218923-24-0
2-(3-(N-benzotriazolcarbonyloxy)(phenyl)(methyl)phenyl) propanoic acid benzotriazolide

: 3332-29-4
O-ethylhydroxylamine hydrochloride

: 1218923-26-2
(3-(1-(ethoxycarbamoyl)ethyl)phenyl)(phenyl)methyl ethoxycarbamate

Guidance literature:: With triethylamine; In toluene; at 20 ℃; for 25h;
DOI:10.1016/j.ejmech.2010.04.008

Reference yield:

: 59960-32-6
Dihydroketoprofen

: 1218923-26-2
(3-(1-(ethoxycarbamoyl)ethyl)phenyl)(phenyl)methyl ethoxycarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / toluene / 1 h / 20 °C

2: triethylamine / toluene / 25 h / 20 °C

With triethylamine; In toluene;
DOI:10.1007/s00044-010-9309-2

Reference yield:

: 22071-15-4,22161-86-0
ketoprofen

: 1218923-26-2
(3-(1-(ethoxycarbamoyl)ethyl)phenyl)(phenyl)methyl ethoxycarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: palladium on activated charcoal; hydrogen / tetrahydrofuran

2: triethylamine / toluene / 1 h / 20 °C

3: triethylamine / toluene / 25 h / 20 °C

With palladium on activated charcoal; hydrogen; triethylamine; In tetrahydrofuran; toluene;
DOI:10.1007/s00044-010-9309-2