2-(3-(N-benzotriazolcarbonyloxy)(phenyl)(methyl)phenyl) propanoic acid benzotriazolide

Base Information

Chemical Name:2-(3-(N-benzotriazolcarbonyloxy)(phenyl)(methyl)phenyl) propanoic acid benzotriazolide
CAS No.:1218923-24-0
Molecular Formula:C₂₉H₂₂N₆O₃
Molecular Weight:502.532
Hs Code.:

Synonyms:2-(3-(N-benzotriazolcarbonyloxy)(phenyl)(methyl)phenyl) propanoic acid benzotriazolide

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Chemical Property of 2-(3-(N-benzotriazolcarbonyloxy)(phenyl)(methyl)phenyl) propanoic acid benzotriazolide

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Technology Process of 2-(3-(N-benzotriazolcarbonyloxy)(phenyl)(methyl)phenyl) propanoic acid benzotriazolide

There total 2 articles about 2-(3-(N-benzotriazolcarbonyloxy)(phenyl)(methyl)phenyl) propanoic acid benzotriazolide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 59960-32-6
Dihydroketoprofen

: 65095-13-8
1-benzotriazolecarboxylic acid chloride

: 1218923-24-0
2-(3-(N-benzotriazolcarbonyloxy)(phenyl)(methyl)phenyl) propanoic acid benzotriazolide

Guidance literature:: With triethylamine; In toluene; at 20 ℃;
DOI:10.1016/j.ejmech.2010.04.008

Reference yield:

: 22071-15-4,22161-86-0
ketoprofen

: 1218923-24-0
2-(3-(N-benzotriazolcarbonyloxy)(phenyl)(methyl)phenyl) propanoic acid benzotriazolide

Guidance literature:: Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / tetrahydrofuran

2: triethylamine / toluene / 1 h / 20 °C

With palladium on activated charcoal; hydrogen; triethylamine; In tetrahydrofuran; toluene;
DOI:10.1007/s00044-010-9309-2