2-bis-Δ^8,13-bicyclohomofarnezenoylaminopyrimidine

Base Information

Chemical Name:2-bis-Δ^8,13-bicyclohomofarnezenoylaminopyrimidine
CAS No.:1424348-23-1
Molecular Formula:C₃₆H₅₃N₃O₂
Molecular Weight:559.836
Hs Code.:

2-bis-Δ<sup>8,13</sup>-bicyclohomofarnezenoylaminopyrimidine

Synonyms:2-bis-Δ^8,13-bicyclohomofarnezenoylaminopyrimidine

Suppliers and Price of 2-bis-Δ^8,13-bicyclohomofarnezenoylaminopyrimidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-bis-Δ^8,13-bicyclohomofarnezenoylaminopyrimidine

Chemical Property:

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Technology Process of 2-bis-Δ^8,13-bicyclohomofarnezenoylaminopyrimidine

There total 7 articles about 2-bis-Δ^8,13-bicyclohomofarnezenoylaminopyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 109-12-6
2-aminopyrimidine

: 29065-24-5
2-((1S, 4aS, 8aS)-5,5,8a-trimethyl-2-methylenedecahydronaphthalen-1-yl)acetic acid

: 538-75-0
dicyclohexyl-carbodiimide

: 1424348-29-7
Δ^8,13-bicyclohomofarnezenic acid N-(pyrimidin-2-yl)amide

: 1424348-23-1
2-bis-Δ^8,13-bicyclohomofarnezenoylaminopyrimidine

: 1424348-25-3
N-Δ^8,13-bicyclohomofarnezenoyl-N,N′-dicyclohexylurea

: 2387-23-7
1,3-Dicyclohexylurea

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1055/s-0032-1318253

Reference yield: 22.0%

: 109-12-6
2-aminopyrimidine

: 29065-24-5
2-((1S, 4aS, 8aS)-5,5,8a-trimethyl-2-methylenedecahydronaphthalen-1-yl)acetic acid

: 1424348-29-7
Δ^8,13-bicyclohomofarnezenic acid N-(pyrimidin-2-yl)amide

: 1424348-23-1
2-bis-Δ^8,13-bicyclohomofarnezenoylaminopyrimidine

: 1424348-25-3
N-Δ^8,13-bicyclohomofarnezenoyl-N,N′-dicyclohexylurea

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 15h; Reflux;
DOI:10.1007/s00044-013-0720-3

Reference yield:

: 564-20-5,1216-84-8,30450-17-0,58976-28-6,64090-92-2,67844-42-2,79768-41-5,79768-42-6,86688-27-9,86688-28-0,95406-08-9,98719-44-9,98719-46-1,131831-65-7,140851-80-5
(3aR)-(+)-sclareolide

: 1424348-29-7
Δ^8,13-bicyclohomofarnezenic acid N-(pyrimidin-2-yl)amide

: 1424348-23-1
2-bis-Δ^8,13-bicyclohomofarnezenoylaminopyrimidine

: 1424348-25-3
N-Δ^8,13-bicyclohomofarnezenoyl-N,N′-dicyclohexylurea

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium aluminium tetrahydride / diethyl ether / 2 h / Heating

2.1: pyridine / 2 h / 20 °C

3.1: pyridine; trichlorophosphate / 5 h / 0 - 24 °C

3.2: monoperftalic acid / 5 h / 0 °C

4.1: potassium hydroxide / methanol / 2 h / 20 °C

5.1: Jones reagent / acetone / 3 h / 20 °C

6.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 15 h / Reflux

With pyridine; dmap; lithium aluminium tetrahydride; Jones reagent; dicyclohexyl-carbodiimide; potassium hydroxide; trichlorophosphate; In methanol; diethyl ether; dichloromethane; acetone;
DOI:10.1007/s00044-013-0720-3