-p-chlorobenzene

Base Information

• Chemical Name: -p-chlorobenzene
• CAS No.: 73178-07-1
• Molecular Formula: C₁₃H₁₂ClIO₄S
• Molecular Weight: 426.659

Synonyms:-p-chlorobenzene

Chemical Property of -p-chlorobenzene

Chemical Property:

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Technology Process of -p-chlorobenzene

There total 8 articles about -p-chlorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

4-chloro-1-(diacetoxyiodo)benzene (6973-73-5) + p-toluenesulfonic acid monohydrate (6192-52-5) → -p-chlorobenzene (73178-07-1)

Guidance literature:

for 0.00555556h; Microwave irradiation; neat (no solvent);

DOI:10.3184/030823409X396427

Reference yield: 96.0%

1-Chloro-4-iodobenzene (637-87-6) + toluene-4-sulfonic acid (104-15-4) → -p-chlorobenzene (73178-07-1)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; at 20 ℃; for 2h;

DOI:10.1055/s-2005-872697

Reference yield: 82.3%

1-Chloro-4-iodobenzene (637-87-6) + -o-toluene (73177-97-6) → -p-chlorobenzene (73178-07-1)

Guidance literature:

In dichloromethane; for 72h; Ambient temperature;

DOI:10.1021/jo00163a022

upstream raw materials:

1-Chloro-4-iodobenzene

[hydroxy(tosyloxy)iodo]benzene

-o-toluene

1-chloro-4-iodosylbenzene

Downstream raw materials:

(p-chlorophenyl)(5-methyl-2-thienyl)iodonium tosylate

(p-chlorophenyl)(5-ethyl-2-thienyl)iodonium tosylate

Toluene-4-sulfonate(4-chloro-phenyl)-furan-2-yl-iodonium;

(p-chlorophenyl)(3-methyl-2-thienyl)iodonium tosylate

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