2,3,5,6-Tetramethoxy-benzoylchlorid

Base Information

Chemical Name:2,3,5,6-Tetramethoxy-benzoylchlorid
CAS No.:6172-66-3
Molecular Formula:C₁₁H₁₃ClO₅
Molecular Weight:260.674
Hs Code.:

Synonyms:2,3,5,6-Tetramethoxy-benzoylchlorid

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Chemical Property of 2,3,5,6-Tetramethoxy-benzoylchlorid

Chemical Property:

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Technology Process of 2,3,5,6-Tetramethoxy-benzoylchlorid

There total 5 articles about 2,3,5,6-Tetramethoxy-benzoylchlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2441-46-5
1,2,4,5-tetramethoxybenzene

: 6172-66-3
2,3,5,6-Tetramethoxy-benzoylchlorid

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / Inert atmosphere

1.2: Inert atmosphere

2.1: sodium chlorite; aminosulfonic acid / tetrahydrofuran; water; dimethyl sulfoxide / Inert atmosphere

3.1: thionyl chloride / 2 h / Inert atmosphere; Reflux

With sodium chlorite; n-butyllithium; thionyl chloride; aminosulfonic acid; In tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1139/v11-087

Reference yield:

: 20491-91-2
2,4,5-trimethoxyphenol

: 6172-66-3
2,3,5,6-Tetramethoxy-benzoylchlorid

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide / tetrahydrofuran; water / Inert atmosphere

2.1: n-butyllithium / Inert atmosphere

2.2: Inert atmosphere

3.1: sodium chlorite; aminosulfonic acid / tetrahydrofuran; water; dimethyl sulfoxide / Inert atmosphere

4.1: thionyl chloride / 2 h / Inert atmosphere; Reflux

With sodium chlorite; n-butyllithium; thionyl chloride; aminosulfonic acid; potassium hydroxide; In tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1139/v11-087

Reference yield:

: 30225-87-7
2,4,5-trimethoxyphenyl formate

: 6172-66-3
2,3,5,6-Tetramethoxy-benzoylchlorid

Guidance literature:: Multi-step reaction with 5 steps

1.1: water; potassium hydroxide / tetrahydrofuran / Inert atmosphere

2.1: potassium hydroxide / tetrahydrofuran; water / Inert atmosphere

3.1: n-butyllithium / Inert atmosphere

3.2: Inert atmosphere

4.1: sodium chlorite; aminosulfonic acid / tetrahydrofuran; water; dimethyl sulfoxide / Inert atmosphere

5.1: thionyl chloride / 2 h / Inert atmosphere; Reflux

With sodium chlorite; n-butyllithium; thionyl chloride; aminosulfonic acid; water; potassium hydroxide; In tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1139/v11-087