N-Isopropyl-2-{3-[3-(3-nitro-phenyl)-ureido]-2,4-dioxo-5-phenyl-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl}-N-phenyl-acetamide

Base Information

Chemical Name:N-Isopropyl-2-{3-[3-(3-nitro-phenyl)-ureido]-2,4-dioxo-5-phenyl-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl}-N-phenyl-acetamide
CAS No.:184945-28-6
Molecular Formula:C₃₃H₃₀N₆O₆
Molecular Weight:606.638
Hs Code.:

Synonyms:N-Isopropyl-2-{3-[3-(3-nitro-phenyl)-ureido]-2,4-dioxo-5-phenyl-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl}-N-phenyl-acetamide

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Chemical Property of N-Isopropyl-2-{3-[3-(3-nitro-phenyl)-ureido]-2,4-dioxo-5-phenyl-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl}-N-phenyl-acetamide

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Technology Process of N-Isopropyl-2-{3-[3-(3-nitro-phenyl)-ureido]-2,4-dioxo-5-phenyl-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl}-N-phenyl-acetamide

There total 5 articles about N-Isopropyl-2-{3-[3-(3-nitro-phenyl)-ureido]-2,4-dioxo-5-phenyl-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl}-N-phenyl-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 161455-97-6
2-bromo-N-isopropyl-N-phenyl-acetamide

: 184945-28-6
N-Isopropyl-2-{3-[3-(3-nitro-phenyl)-ureido]-2,4-dioxo-5-phenyl-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl}-N-phenyl-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 10.0 g / K₂CO₃ / dimethylformamide

2: 7.5 g / tetrahydrofuran / 4 h / Ambient temperature

3: 6.3 g / Zn, glacial AcOH / 1 h / Ambient temperature

4: 335 mg / a) CH₂Cl₂, RT, 20 min, b) CH₃CN, reflux, 30 min

With potassium carbonate; acetic acid; zinc; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm9601664

Reference yield:

: 161455-90-9
N-isopropyl-N-phenyl-2-(2-phenylamino-phenylamino)-acetamide

: 184945-28-6
N-Isopropyl-2-{3-[3-(3-nitro-phenyl)-ureido]-2,4-dioxo-5-phenyl-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl}-N-phenyl-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 7.5 g / tetrahydrofuran / 4 h / Ambient temperature

2: 6.3 g / Zn, glacial AcOH / 1 h / Ambient temperature

3: 335 mg / a) CH₂Cl₂, RT, 20 min, b) CH₃CN, reflux, 30 min

With acetic acid; zinc; In tetrahydrofuran;
DOI:10.1021/jm9601664

Reference yield:

: 534-85-0
N-phenyl-1,2-benzenediamine

: 184945-28-6
N-Isopropyl-2-{3-[3-(3-nitro-phenyl)-ureido]-2,4-dioxo-5-phenyl-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl}-N-phenyl-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: 10.0 g / K₂CO₃ / dimethylformamide

2: 7.5 g / tetrahydrofuran / 4 h / Ambient temperature

3: 6.3 g / Zn, glacial AcOH / 1 h / Ambient temperature

4: 335 mg / a) CH₂Cl₂, RT, 20 min, b) CH₃CN, reflux, 30 min

With potassium carbonate; acetic acid; zinc; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm9601664