1-(4-cyclopropyl-3,4-dihydroquinoxalin-1(2H)-yl)-2-(2,5-dichlorophenoxy)ethanone trifluoroacetate

Base Information

Chemical Name:1-(4-cyclopropyl-3,4-dihydroquinoxalin-1(2H)-yl)-2-(2,5-dichlorophenoxy)ethanone trifluoroacetate
CAS No.:1445980-92-6
Molecular Formula:C₂HF₃O₂*C₁₉H₁₈Cl₂N₂O₂
Molecular Weight:491.294
Hs Code.:

Synonyms:1-(4-cyclopropyl-3,4-dihydroquinoxalin-1(2H)-yl)-2-(2,5-dichlorophenoxy)ethanone trifluoroacetate

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Chemical Property of 1-(4-cyclopropyl-3,4-dihydroquinoxalin-1(2H)-yl)-2-(2,5-dichlorophenoxy)ethanone trifluoroacetate

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Technology Process of 1-(4-cyclopropyl-3,4-dihydroquinoxalin-1(2H)-yl)-2-(2,5-dichlorophenoxy)ethanone trifluoroacetate

There total 7 articles about 1-(4-cyclopropyl-3,4-dihydroquinoxalin-1(2H)-yl)-2-(2,5-dichlorophenoxy)ethanone trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1224640-13-4
1-cyclopropyl-1,2,3,4-tetrahydro-quinoxaline

: 582-54-7
2,5-dichlorophenoxyacetic acid

: 76-05-1
trifluoroacetic acid

: 1445980-92-6
1-(4-cyclopropyl-3,4-dihydroquinoxalin-1(2H)-yl)-2-(2,5-dichlorophenoxy)ethanone trifluoroacetate

Guidance literature:: 1-cyclopropyl-1,2,3,4-tetrahydro-quinoxaline; 2,5-dichlorophenoxyacetic acid; With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 25 ℃; for 2h;

trifluoroacetic acid;

Reference yield:

: 1224640-11-2
1-cyclopropyl-4-hydroxy-1,2,3,4-tetrahydroquinoxaline-2,3-dione

: 1445980-92-6
1-(4-cyclopropyl-3,4-dihydroquinoxalin-1(2H)-yl)-2-(2,5-dichlorophenoxy)ethanone trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine / N,N-dimethyl-formamide / 2 h / 135 °C / Inert atmosphere

2: borane-THF / tetrahydrofuran / 4 h / 50 °C

3: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 2 h / 25 °C

With borane-THF; N-ethyl-N,N-diisopropylamine; triphenylphosphine; HATU; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 1224640-12-3
1-cyclopropyl-1,2,3,4-tetrahydroquinoxaline-2,3-dione

: 1445980-92-6
1-(4-cyclopropyl-3,4-dihydroquinoxalin-1(2H)-yl)-2-(2,5-dichlorophenoxy)ethanone trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: borane-THF / tetrahydrofuran / 4 h / 50 °C

2: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 2 h / 25 °C

With borane-THF; N-ethyl-N,N-diisopropylamine; HATU; In tetrahydrofuran; N,N-dimethyl-formamide;