1-diazo-4-(4-methoxyphenyl)-1-(triethylsilyl)-4-(triethyl silyloxy) butan-2-one

Base Information

Chemical Name:1-diazo-4-(4-methoxyphenyl)-1-(triethylsilyl)-4-(triethyl silyloxy) butan-2-one
CAS No.:1411737-01-3
Molecular Formula:C₂₃H₄₀N₂O₃Si₂
Molecular Weight:448.753
Hs Code.:

Synonyms:1-diazo-4-(4-methoxyphenyl)-1-(triethylsilyl)-4-(triethyl silyloxy) butan-2-one

Suppliers and Price of 1-diazo-4-(4-methoxyphenyl)-1-(triethylsilyl)-4-(triethyl silyloxy) butan-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-diazo-4-(4-methoxyphenyl)-1-(triethylsilyl)-4-(triethyl silyloxy) butan-2-one

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Technology Process of 1-diazo-4-(4-methoxyphenyl)-1-(triethylsilyl)-4-(triethyl silyloxy) butan-2-one

There total 1 articles about 1-diazo-4-(4-methoxyphenyl)-1-(triethylsilyl)-4-(triethyl silyloxy) butan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 994-30-9
triethylsilyl chloride

: 61861-17-4
α-triethylsilyl-α-diazoacetone

: 123-11-5
4-methoxy-benzaldehyde

: 1411737-01-3
1-diazo-4-(4-methoxyphenyl)-1-(triethylsilyl)-4-(triethyl silyloxy) butan-2-one

Guidance literature:: α-triethylsilyl-α-diazoacetone; With potassium hexamethylsilazane; In toluene; at -78 ℃; for 0.166667h; Inert atmosphere;

triethylsilyl chloride; 4-methoxy-benzaldehyde; In toluene; at -78 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tet.2012.09.063