benzyl (3S,4S)-3-fluoro-4-((4-nitrobenzoyl)oxy)piperidine-1-carboxylate

Base Information

• Chemical Name: benzyl (3S,4S)-3-fluoro-4-((4-nitrobenzoyl)oxy)piperidine-1-carboxylate
• CAS No.: 1209780-78-8
• Molecular Formula: C₁₃H₁₆FNO₃
• Molecular Weight: 253.273

Synonyms:benzyl (3S,4S)-3-fluoro-4-((4-nitrobenzoyl)oxy)piperidine-1-carboxylate

Chemical Property of benzyl (3S,4S)-3-fluoro-4-((4-nitrobenzoyl)oxy)piperidine-1-carboxylate

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

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Technology Process of benzyl (3S,4S)-3-fluoro-4-((4-nitrobenzoyl)oxy)piperidine-1-carboxylate

There total 7 articles about benzyl (3S,4S)-3-fluoro-4-((4-nitrobenzoyl)oxy)piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl trans-3-fluoro-4-((4-nitrobenzoyl)oxy)piperidine-1-carboxylate → benzyl (3R,4R)-3-fluoro-4-((4-nitrobenzoyl)oxy)piperidine-1-carboxylate (913574-95-5,913574-96-6,1554141-63-7) + benzyl (3S,4S)-3-fluoro-4-((4-nitrobenzoyl)oxy)piperidine-1-carboxylate (1209780-78-8,913574-95-5,913574-96-6,1554141-63-7)

Guidance literature:

With potassium carbonate; In methanol; at 20 ℃; for 15h;

Reference yield:

benzyl trans-3-fluoro-4-hydroxypiperidine-1-carboxylate (913574-95-5,913574-96-6,1554141-63-7) → benzyl (3R,4R)-3-fluoro-4-((4-nitrobenzoyl)oxy)piperidine-1-carboxylate (913574-95-5,913574-96-6,1554141-63-7) + benzyl (3S,4S)-3-fluoro-4-((4-nitrobenzoyl)oxy)piperidine-1-carboxylate (1209780-78-8,913574-95-5,913574-96-6,1554141-63-7)

Guidance literature:

With carbon dioxide; diethylamine; In ethanol;

Reference yield:

benzyl 3-fluoro-4-oxopiperidine-1-carboxylate (845256-59-9) → benzyl (3S,4S)-3-fluoro-4-((4-nitrobenzoyl)oxy)piperidine-1-carboxylate (1209780-78-8,913574-95-5,913574-96-6,1554141-63-7)

Guidance literature:

With sodium tetrahydroborate; In ethanol; for 0.5h;

upstream raw materials:

benzyl 4-oxo-1-piperidinecarboxylate

benzyl 3-fluoro-4-oxopiperidine-1-carboxylate

phenylmethyl 4-[(trimethylsilyl)oxy]-3,6-dihydro-1(2H)-pyridinecarboxylate

benzyl cis-3-fluoro-4-hydroxypiperidine-1-carboxylate

Downstream raw materials:

(3S,4S)-3-fluoropiperidin-4-ol

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