benzyl 4-(triMethylsilylo×y)-5,6-dihydropyridine-1(2H)-carbo×ylate

Base Information

Chemical Name:benzyl 4-(triMethylsilylo×y)-5,6-dihydropyridine-1(2H)-carbo×ylate
CAS No.:1147998-34-2
Molecular Formula:C16H23NO3Si
Molecular Weight:305.449
Hs Code.:2933399090
Mol file:1147998-34-2.mol

Synonyms:benzyl 4-(triMethylsilylo×y)-5,6-dihydropyridine-1(2H)-carbo×ylate;Benzyl 4-((triMethylsilyl)oxy)-5,6-dihydropyridine-1(2H)-carboxylate

Suppliers and Price of benzyl 4-(triMethylsilylo×y)-5,6-dihydropyridine-1(2H)-carbo×ylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Benzyl4-((trimethylsilyl)oxy)-5,6-dihydropyridine-1(2H)-carboxylate 95+%
1g
$ 329.00

Chemenu
benzyl4-((trimethylsilyl)oxy)-3,6-dihydropyridine-1(2H)-carboxylate 95%
1g
$ 310.00

American Custom Chemicals Corporation
BENZYL-4-((TRIMETHYLSILYL)OXY)-5,6-DIHYDROPYRIDINE-1(2H)-CARBOXYLATE 95.00%
1G
$ 735.00

Alichem
Benzyl4-((trimethylsilyl)oxy)-5,6-dihydropyridine-1(2H)-carboxylate
1g
$ 400.00

Total 12 raw suppliers

Chemical Property of benzyl 4-(triMethylsilylo×y)-5,6-dihydropyridine-1(2H)-carbo×ylate

Chemical Property:

PSA：38.77000
LogP:3.70220
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Benzyl4-((trimethylsilyl)oxy)-5,6-dihydropyridine-1(2H)-carboxylate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of benzyl 4-(triMethylsilylo×y)-5,6-dihydropyridine-1(2H)-carbo×ylate

There total 3 articles about benzyl 4-(triMethylsilylo×y)-5,6-dihydropyridine-1(2H)-carbo×ylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 75-77-4
chloro-trimethyl-silane

: 19099-93-5
benzyl 4-oxo-1-piperidinecarboxylate

: 1147998-34-2
phenylmethyl 4-[(trimethylsilyl)oxy]-3,6-dihydro-1(2H)-pyridinecarboxylate

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 80 ℃; for 16h;

Reference yield:

: 19099-93-5
benzyl 4-oxo-1-piperidinecarboxylate

: 1147998-34-2
phenylmethyl 4-[(trimethylsilyl)oxy]-3,6-dihydro-1(2H)-pyridinecarboxylate

Guidance literature:: benzyl 4-oxo-1-piperidinecarboxylate; With triethylamine; In N,N-dimethyl-formamide; at 80 ℃; for 18h;

With chloro-trimethyl-silane; at 80 ℃; for 18h;

Reference yield:

: 6099-86-1
cyclohexylmethyl chlorocarbonate

: 1147998-34-2
phenylmethyl 4-[(trimethylsilyl)oxy]-3,6-dihydro-1(2H)-pyridinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / tetrahydrofuran; water / 2.33 h / -5 - 20 °C

2: triethylamine / N,N-dimethyl-formamide / 85 °C

With potassium carbonate; triethylamine; In tetrahydrofuran; water; N,N-dimethyl-formamide;