Technology Process of C34H22BBrN4O3
There total 4 articles about C34H22BBrN4O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C32H34BBrN4; 4-nitro-benzoyl chloride;
In
1,2-dichloro-benzene;
at 150 ℃;
for 0.5h;
Inert atmosphere;
With
pyridine;
In
1,2-dichloro-benzene;
for 1h;
Reflux;
methanol;
Further stages;
DOI:10.1002/ejoc.201402435
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: phenylmagnesium bromide / tetrahydrofuran / 0.5 h / Inert atmosphere
1.2: -93 - 20 °C / Inert atmosphere
2.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 1 h / 20 °C / Inert atmosphere
2.2: 0.25 h / 0 °C / Inert atmosphere
3.1: 1,2-dichloro-benzene / 2 h / 150 °C / Inert atmosphere
4.1: 1,2-dichloro-benzene / 0.5 h / 150 °C / Inert atmosphere
4.2: air / 1 h / Reflux
With
sodium tetrahydroborate; phenylmagnesium bromide;
In
tetrahydrofuran; methanol; 1,2-dichloro-benzene;
DOI:10.1002/ejoc.201402435
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: phenylmagnesium bromide / tetrahydrofuran / 0.5 h / Inert atmosphere
1.2: -93 - 20 °C / Inert atmosphere
2.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 1 h / 20 °C / Inert atmosphere
2.2: 0.25 h / 0 °C / Inert atmosphere
3.1: 1,2-dichloro-benzene / 2 h / 150 °C / Inert atmosphere
4.1: 1,2-dichloro-benzene / 0.5 h / 150 °C / Inert atmosphere
4.2: air / 1 h / Reflux
With
sodium tetrahydroborate; phenylmagnesium bromide;
In
tetrahydrofuran; methanol; 1,2-dichloro-benzene;
DOI:10.1002/ejoc.201402435
