4-(4-Bromophenylsulfonyl)piperidine

Base Information

Chemical Name:4-(4-Bromophenylsulfonyl)piperidine
CAS No.:285995-01-9
Molecular Formula:C₁₁H₁₄BrNO₂S
Molecular Weight:304.208
Hs Code.:
European Community (EC) Number:829-363-0
Mol file:285995-01-9.mol

Synonyms:4-(4-bromophenylsulfonyl)piperidine;285995-01-9;4-(4-bromophenyl)sulfonylpiperidine;SCHEMBL5212189;JLFNPSVUHQMQHA-UHFFFAOYSA-N;4-(4-Bromophenylsulphonyl)piperidine;4-(4-BROMOBENZENESULFONYL)PIPERIDINE;EN300-241634

Suppliers and Price of 4-(4-Bromophenylsulfonyl)piperidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4-[(4-BROMOPHENYL)SULFONYL]PIPERIDINE 95.00%
5MG
$ 500.03

AK Scientific
4-(4-Bromophenylsulfonyl)piperidine
2.5g
$ 625.00

Total 3 raw suppliers

Chemical Property of 4-(4-Bromophenylsulfonyl)piperidine

Chemical Property:

Boiling Point:447.4±45.0 °C(Predicted)
PKA:9.19±0.10(Predicted)
Density:1.477±0.06 g/cm3(Predicted)
XLogP3:2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:302.99286
Heavy Atom Count:16
Complexity:311

Purity/Quality:

99% ^*data from raw suppliers

4-[(4-BROMOPHENYL)SULFONYL]PIPERIDINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CNCCC1S(=O)(=O)C2=CC=C(C=C2)Br

Technology Process of 4-(4-Bromophenylsulfonyl)piperidine

There total 4 articles about 4-(4-Bromophenylsulfonyl)piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 226398-62-5
4-(4-bromobenzenesulfonyl)piperidine-1-carboxylic acid tert-butyl ester

: 285995-01-9
4-(4-bromophenylsulfonyl)piperidine

Guidance literature:: With hydrogenchloride; In methanol; for 3h; Heating;
DOI:10.1021/jm011030v

Reference yield:

: 106-53-6
para-bromobenzenethiol

: 285995-01-9
4-(4-bromophenylsulfonyl)piperidine

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / K₂CO₃ / acetonitrile / 18 h / Heating

2: 69 percent / oxone; Al₂O₃ / CHCl₃; H₂O / 18 h / Heating

3: 5 N aq. HCl / methanol / 3 h / Heating

With hydrogenchloride; aluminum oxide; Oxone; potassium carbonate; In methanol; chloroform; water; acetonitrile;
DOI:10.1021/jm011030v

Reference yield:

: 141699-59-4
1-(tert-butoxycarbonyl)piperidin-4-yl methanesulfonate

: 285995-01-9
4-(4-bromophenylsulfonyl)piperidine

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / K₂CO₃ / acetonitrile / 18 h / Heating

2: 69 percent / oxone; Al₂O₃ / CHCl₃; H₂O / 18 h / Heating

3: 5 N aq. HCl / methanol / 3 h / Heating

With hydrogenchloride; aluminum oxide; Oxone; potassium carbonate; In methanol; chloroform; water; acetonitrile;
DOI:10.1021/jm011030v