(-)-(1R,2S,5R)-8-phenylmenthyl 3-((4R,5S)-1-tert-butoxycarbonyl-4,5-dihydro-4-phenyl-5-trimethylsilyl-1H-pyrazole)carboxylate

Base Information

Chemical Name:(-)-(1R,2S,5R)-8-phenylmenthyl 3-((4R,5S)-1-tert-butoxycarbonyl-4,5-dihydro-4-phenyl-5-trimethylsilyl-1H-pyrazole)carboxylate
CAS No.:196314-29-1
Molecular Formula:C₃₄H₄₈N₂O₄Si
Molecular Weight:576.852
Hs Code.:

Synonyms:(-)-(1R,2S,5R)-8-phenylmenthyl 3-((4R,5S)-1-tert-butoxycarbonyl-4,5-dihydro-4-phenyl-5-trimethylsilyl-1H-pyrazole)carboxylate

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Chemical Property of (-)-(1R,2S,5R)-8-phenylmenthyl 3-((4R,5S)-1-tert-butoxycarbonyl-4,5-dihydro-4-phenyl-5-trimethylsilyl-1H-pyrazole)carboxylate

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Technology Process of (-)-(1R,2S,5R)-8-phenylmenthyl 3-((4R,5S)-1-tert-butoxycarbonyl-4,5-dihydro-4-phenyl-5-trimethylsilyl-1H-pyrazole)carboxylate

There total 4 articles about (-)-(1R,2S,5R)-8-phenylmenthyl 3-((4R,5S)-1-tert-butoxycarbonyl-4,5-dihydro-4-phenyl-5-trimethylsilyl-1H-pyrazole)carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119240-64-1
(1'R,2'S,5'R)-2'-(2''-phenylpropan-2''-yl)-5'-methylcyclohexyl (E)-3-phenylpropenoate

: 196314-29-1
(-)-(1R,2S,5R)-8-phenylmenthyl 3-((4R,5S)-1-tert-butoxycarbonyl-4,5-dihydro-4-phenyl-5-trimethylsilyl-1H-pyrazole)carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: hexane; tetrahydrofuran / 192 h / 67 °C

2: NEt₃, DMAP / hexane; tetrahydrofuran / 2 h / Ambient temperature

With dmap; triethylamine; In tetrahydrofuran; hexane;
DOI:10.1002/(SICI)1521-3765(19990301)5:3<883::AID-CHEM883>3.0.CO;2-0

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 4-Phenyl-5-trimethylsilanyl-4,5-dihydro-1H-pyrazole-3-carboxylic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

: 196314-29-1
(-)-(1R,2S,5R)-8-phenylmenthyl 3-((4R,5S)-1-tert-butoxycarbonyl-4,5-dihydro-4-phenyl-5-trimethylsilyl-1H-pyrazole)carboxylate

: (-)-(1R,2S,5R)-8-phenylmenthyl 3-((4S,5R)-1-tert-butoxycarbonyl-4,5-dihydro-4-phenyl-5-trimethylsilyl-1H-pyrazole)carboxylate

Guidance literature:: With dmap; triethylamine; In tetrahydrofuran; hexane; for 2h; Yield given; Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;
DOI:10.1002/(SICI)1521-3765(19990301)5:3<883::AID-CHEM883>3.0.CO;2-0