dimethyl 1-benzyl-1,4-dihydro-4-(4-methoxyphenyl)pyridine-3,5-dicarboxylate

Base Information

• Chemical Name: dimethyl 1-benzyl-1,4-dihydro-4-(4-methoxyphenyl)pyridine-3,5-dicarboxylate
• CAS No.: 200628-26-8
• Molecular Formula: C₂₃H₂₃NO₅
• Molecular Weight: 393.439

Synonyms:dimethyl 1-benzyl-1,4-dihydro-4-(4-methoxyphenyl)pyridine-3,5-dicarboxylate

Chemical Property of dimethyl 1-benzyl-1,4-dihydro-4-(4-methoxyphenyl)pyridine-3,5-dicarboxylate

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Technology Process of dimethyl 1-benzyl-1,4-dihydro-4-(4-methoxyphenyl)pyridine-3,5-dicarboxylate

There total 1 articles about dimethyl 1-benzyl-1,4-dihydro-4-(4-methoxyphenyl)pyridine-3,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-methoxy-benzaldehyde (123-11-5) + propynoic acid methyl ester (922-67-8) + benzylamine (100-46-9) → dimethyl 1-benzyl-1,4-dihydro-4-(4-methoxyphenyl)pyridine-3,5-dicarboxylate (200628-26-8)

Guidance literature:

With silica gel; for 0.0666667h; microwave irradiation;

DOI:10.1007/s007060170012

Reference yield: 73.0%

dimethyl 1-benzyl-1,4-dihydro-4-(4-methoxyphenyl)pyridine-3,5-dicarboxylate (200628-26-8) → tetramethyl 1,5-dibenzyl-1,5,8,8bα-tetrahydro-4,8-bis(4-methoxyphenyl)cyclobuta[1,2-b:3,4-b']dipyridine-3,4aα,7,8aβ(4H,4bβH)-tetracarboxylate + tetramethyl 3,9-dibenzyl-6,12-bis(4-methoxyphenyl)-3,9-diazahexacyclo[6.4.0.02.7.04.11.05.10]dodecane-1,5,7,11-tetracarboxylate

Guidance literature:

In tetrahydrofuran; methanol; for 672000h; UV-irradiation;

DOI:10.1002/(SICI)1099-0690(200001)2000:2<245::AID-EJOC245>3.0.CO;2-2

Reference yield: 37.0%

dimethyl 1-benzyl-1,4-dihydro-4-(4-methoxyphenyl)pyridine-3,5-dicarboxylate (200628-26-8) → tetramethyl 1,5-dibenzyl-1,5,8,8bβ-tetrahydro-4,8-bis(4-methoxyphenyl)cyclobuta[1,2-b:3,4-b']dipyridine-3,4aβ,7,8aβ(4H,4bβH)-tetracarboxylate + tetramethyl 1,5-dibenzyl-1,5,8,8bα-tetrahydro-4,8-bis(4-methoxyphenyl)cyclobuta[1,2-b:3,4-b']dipyridine-3,4aα,7,8aβ(4H,4bβH)-tetracarboxylate

Guidance literature:

In tetrahydrofuran; methanol; for 672000h; Irradiation;

DOI:10.1002/(SICI)1099-0690(200001)2000:2<245::AID-EJOC245>3.0.CO;2-2

upstream raw materials:

4-methoxy-benzaldehyde

propynoic acid methyl ester

benzylamine

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