C₂₉H₃₂NO₂P

Base Information

• Chemical Name: C₂₉H₃₂NO₂P
• CAS No.: 1333420-34-0
• Molecular Formula: C₂₉H₃₂NO₂P
• Molecular Weight: 457.552
• Mol file: 1333420-34-0.mol

Synonyms:C₂₉H₃₂NO₂P

Chemical Property of C₂₉H₃₂NO₂P

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₂₉H₃₂NO₂P

There total 1 articles about C₂₉H₃₂NO₂P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

1-Adamantanamine (768-94-5) + 2,3-dimethoxyphenyldiphenylphosphine oxide (404868-18-4) → C29H32NO2P (1333420-34-0)

Guidance literature:

1-Adamantanamine; With n-butyllithium; In tetrahydrofuran; hexane; at -80 - 20 ℃; for 2.83333h;

2,3-dimethoxyphenyldiphenylphosphine oxide; In tetrahydrofuran; hexane; at 20 ℃; for 18h;

DOI:10.1002/ejoc.201100769

Reference yield: 97.0%

C29H32NO2P (1333420-34-0) + methyl iodide (74-88-4) → C30H34NO2P (1333420-37-3)

Guidance literature:

With potassium carbonate; In acetonitrile; at 20 ℃; for 40h;

DOI:10.1002/ejoc.201100769

Reference yield: 87.0%

C29H32NO2P (1333420-34-0) + Cinnamyl bromide (4392-24-9) → N-[2'-(diphenylphosphinyl)-6'-methoxylphenyl]-N-cinnamyladamantanamine

Guidance literature:

With potassium carbonate; In acetonitrile; at 80 ℃; for 38h;

DOI:10.1039/c6ob01354f

upstream raw materials:

1-Adamantanamine

2,3-dimethoxyphenyldiphenylphosphine oxide

Downstream raw materials:

C₃₀H₃₄NOP

C₃₀H₃₄NO₂P