4-acetyl-1-benzylthio-5-hydroxy-5-methyl-2,3-diphenyl-1,3-cyclopentadiene

Base Information

Chemical Name:4-acetyl-1-benzylthio-5-hydroxy-5-methyl-2,3-diphenyl-1,3-cyclopentadiene
CAS No.:85572-25-4
Molecular Formula:C₂₇H₂₄O₂S
Molecular Weight:412.552
Hs Code.:

Synonyms:4-acetyl-1-benzylthio-5-hydroxy-5-methyl-2,3-diphenyl-1,3-cyclopentadiene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-acetyl-1-benzylthio-5-hydroxy-5-methyl-2,3-diphenyl-1,3-cyclopentadiene

Chemical Property:

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Technology Process of 4-acetyl-1-benzylthio-5-hydroxy-5-methyl-2,3-diphenyl-1,3-cyclopentadiene

There total 4 articles about 4-acetyl-1-benzylthio-5-hydroxy-5-methyl-2,3-diphenyl-1,3-cyclopentadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: benzylthiodiphenylcyclopropenium bromide

: 123-54-6,81235-32-7
acetylacetone

: 85572-25-4
4-acetyl-1-benzylthio-5-hydroxy-5-methyl-2,3-diphenyl-1,3-cyclopentadiene

Guidance literature:: With triethylamine; In benzene; for 0.333333h; Ambient temperature;
DOI:10.1246/cl.1983.155

Reference yield:

: 2570-01-6
2,3-diphenylcyclopropen-1-thione

: 85572-25-4
4-acetyl-1-benzylthio-5-hydroxy-5-methyl-2,3-diphenyl-1,3-cyclopentadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / benzene / 48 h / Ambient temperature

2: 65 percent / Et₃N / benzene / 0.33 h

With triethylamine; In benzene;
DOI:10.1246/bcsj.56.3015

Reference yield:

: 100-39-0
benzyl bromide

: 85572-25-4
4-acetyl-1-benzylthio-5-hydroxy-5-methyl-2,3-diphenyl-1,3-cyclopentadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / benzene / 48 h / Ambient temperature

2: 65 percent / Et₃N / benzene / 0.33 h

With triethylamine; In benzene;
DOI:10.1246/bcsj.56.3015