O-<2,2-bis(phenylthio)-1-phenylpropyl> S-methyl dithiocarbonate

Base Information

• Chemical Name: O-<2,2-bis(phenylthio)-1-phenylpropyl> S-methyl dithiocarbonate
• CAS No.: 121410-99-9
• Molecular Formula: C₂₃H₂₂OS₄
• Molecular Weight: 442.691
• Mol file: 121410-99-9.mol

Synonyms:O-<2,2-bis(phenylthio)-1-phenylpropyl> S-methyl dithiocarbonate

Chemical Property of O-<2,2-bis(phenylthio)-1-phenylpropyl> S-methyl dithiocarbonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O-<2,2-bis(phenylthio)-1-phenylpropyl> S-methyl dithiocarbonate

There total 3 articles about O-<2,2-bis(phenylthio)-1-phenylpropyl> S-methyl dithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(phenylthio)methane (3561-67-9) → O-<2,2-bis(phenylthio)-1-phenylpropyl> S-methyl dithiocarbonate (121410-99-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) n-BuLi

With n-butyllithium;

DOI:10.1016/S0040-4039(00)82283-2

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + 1,1-bis(phenylthio)ethane (13307-56-7) + benzaldehyde (100-52-7) + methyl iodide (74-88-4) → O-<2,2-bis(phenylthio)-1-phenylpropyl> S-methyl dithiocarbonate (121410-99-9)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1246/bcsj.63.2578

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + Lithium; 2-phenyl-1,1-bis-phenylsulfanyl-propan-2-olate + methyl iodide (74-88-4) → O-<2,2-bis(phenylthio)-1-phenylpropyl> S-methyl dithiocarbonate (121410-99-9)

Guidance literature:

Multistep reaction;

DOI:10.1016/S0040-4039(00)82283-2

upstream raw materials:

carbon disulfide

1,1-bis(phenylthio)ethane

benzaldehyde

methyl iodide

Downstream raw materials:

1-methyl-2-phenylethenyl phenyl sulfide

(Z)-β-phenylthio-β-methylstyrene

phenyl (1E)-1-phenylprop-1-en-2-yl sulfide