Ethyl 2-chloro-2-[(e)-2-(2-nitrophenyl)hydrazono]acetate

Base Information

Chemical Name:Ethyl 2-chloro-2-[(e)-2-(2-nitrophenyl)hydrazono]acetate
CAS No.:37522-26-2
Molecular Formula:C10H10 Cl N3 O4
Molecular Weight:271.66
Hs Code.:
DSSTox Substance ID:DTXSID00421291
Mol file:37522-26-2.mol

Synonyms:37522-26-2;ethyl 2-chloro-2-[(e)-2-(2-nitrophenyl)hydrazono]acetate;ethyl (2E)-2-chloro-2-[(2-nitrophenyl)hydrazinylidene]acetate;11P-035;Ethyl 2-chloro-2-[2-(2-nitrophenyl)hydrazono]acetate;ethyl chloro((2-nitrophenyl)hydrazono)acetate;ETHYL2-CHLORO-2-[2-(2-NITROPHENYL)HYDRAZONO]ACETATE;DTXSID00421291;MFCD00505295;AKOS005078748;A823721;ethyl (Z)-2-chloro-2-(2-(2-nitrophenyl)hydrazono)acetate;2-chloro-2-(2-nitro-phenyl-hydrazono)-acetic acid ethyl ester;ethyl (2E)-2-chloro-2-[2-(2-nitrophenyl)hydrazin-1-ylidene]acetate;ethyl (2E)-2-chloro-2-[(2-nitrophenyl)hydrazono]acetate

Suppliers and Price of Ethyl 2-chloro-2-[(e)-2-(2-nitrophenyl)hydrazono]acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
Ethyl 2-chloro-2-[(E)-2-(2-nitrophenyl)hydrazono]acetate
10mg
$ 146.00

Matrix Scientific
Ethyl 2-chloro-2-[(E)-2-(2-nitrophenyl)hydrazono]acetate
5mg
$ 105.00

Matrix Scientific
Ethyl 2-chloro-2-[(E)-2-(2-nitrophenyl)hydrazono]acetate
1mg
$ 90.00

Crysdot
Ethyl2-chloro-2-[2-(2-nitrophenyl)hydrazono]acetate 95+%
1g
$ 395.00

American Custom Chemicals Corporation
ETHYL 2-CHLORO-2-[(E)-2-(2-NITROPHENYL)HYDRAZONO]ACETATE 95.00%
1G
$ 1091.48

Total 6 raw suppliers

Chemical Property of Ethyl 2-chloro-2-[(e)-2-(2-nitrophenyl)hydrazono]acetate

Chemical Property:

Vapor Pressure:6.12E-06mmHg at 25°C
Boiling Point:378.8°C at 760 mmHg
Flash Point:182.9°C
Density:1.41g/cm³
XLogP3:5.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:5
Exact Mass:271.0359835
Heavy Atom Count:18
Complexity:343

Purity/Quality:

97% ^*data from raw suppliers

Ethyl 2-chloro-2-[(E)-2-(2-nitrophenyl)hydrazono]acetate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(=NNC1=CC=CC=C1[N+](=O)[O-])Cl
Isomeric SMILES:CCOC(=O)/C(=N\NC1=CC=CC=C1[N+](=O)[O-])/Cl

Technology Process of Ethyl 2-chloro-2-[(e)-2-(2-nitrophenyl)hydrazono]acetate

There total 4 articles about Ethyl 2-chloro-2-[(e)-2-(2-nitrophenyl)hydrazono]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 88-74-4
2-nitro-aniline

: 609-15-4
ethyl 2-chloro-3-oxo-butyrate

: 37522-26-2
ethyl [(2-nitrophenyl)hydrazono](chloro)acetate

Guidance literature:: 2-nitro-aniline; With hydrogenchloride; sodium nitrite; In methanol; water; for 0.25h; Cooling with ice;

ethyl 2-chloro-3-oxo-butyrate; In methanol; water; at 0 - 20 ℃; for 1.5h;
DOI:10.1021/acs.joc.9b00716

Reference yield:

: 105-39-5
chloroacetic acid ethyl ester

: 88-74-4
2-nitro-aniline

: 37522-26-2
ethyl [(2-nitrophenyl)hydrazono](chloro)acetate

Guidance literature:: With hydrogenchloride; sodium acetate; sodium nitrite; Multistep reaction; 1.) water; 2.) water, ethanol, 0 - 5 deg C, 3 h -> overnight;