(R)-2-[(1-methoxypropan-2-yl)oxy]phenyl diselenide

Base Information

Chemical Name:(R)-2-[(1-methoxypropan-2-yl)oxy]phenyl diselenide
CAS No.:1264256-07-6
Molecular Formula:C₂₀H₂₆O₄Se₂
Molecular Weight:488.344
Hs Code.:

Synonyms:(R)-2-[(1-methoxypropan-2-yl)oxy]phenyl diselenide

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Chemical Property of (R)-2-[(1-methoxypropan-2-yl)oxy]phenyl diselenide

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Technology Process of (R)-2-[(1-methoxypropan-2-yl)oxy]phenyl diselenide

There total 4 articles about (R)-2-[(1-methoxypropan-2-yl)oxy]phenyl diselenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1264256-01-0
(R)-1-(1-methoxypropan-2-yloxy)benzene

: 1264256-07-6
(R)-2-[(1-methoxypropan-2-yl)oxy]phenyl diselenide

Guidance literature:: (R)-1-(1-methoxypropan-2-yloxy)benzene; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 2.5h; Inert atmosphere;

With selenium; In tetrahydrofuran; hexane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201001272

Reference yield:

: 64658-22-6
(R)-2-phenoxypropan-1-ol

: 1264256-07-6
(R)-2-[(1-methoxypropan-2-yl)oxy]phenyl diselenide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

With n-butyllithium; sodium hydride; In tetrahydrofuran; hexane;
DOI:10.1002/ejoc.201001272

Reference yield:

: 76671-56-2
(R)-2-phenoxypropionic acid ethyl ester

: 1264256-07-6
(R)-2-[(1-methoxypropan-2-yl)oxy]phenyl diselenide

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / -78 - 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / 0 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; n-butyllithium; sodium hydride; In tetrahydrofuran; hexane;
DOI:10.1002/ejoc.201001272