(2-methoxy-2-phenylethyl)(2-{[(R)-1-methoxypropan-2-yl]oxy}phenyl)selane

Base Information

Chemical Name:(2-methoxy-2-phenylethyl)(2-{[(R)-1-methoxypropan-2-yl]oxy}phenyl)selane
CAS No.:1264256-13-4
Molecular Formula:C₁₉H₂₄O₃Se
Molecular Weight:379.358
Hs Code.:

Synonyms:(2-methoxy-2-phenylethyl)(2-{[(R)-1-methoxypropan-2-yl]oxy}phenyl)selane

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Chemical Property of (2-methoxy-2-phenylethyl)(2-{[(R)-1-methoxypropan-2-yl]oxy}phenyl)selane

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Technology Process of (2-methoxy-2-phenylethyl)(2-{[(R)-1-methoxypropan-2-yl]oxy}phenyl)selane

There total 5 articles about (2-methoxy-2-phenylethyl)(2-{[(R)-1-methoxypropan-2-yl]oxy}phenyl)selane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 67-56-1
methanol

: 1264256-07-6
(R)-2-[(1-methoxypropan-2-yl)oxy]phenyl diselenide

: 1264256-13-4
(2-methoxy-2-phenylethyl)(2-{[(R)-1-methoxypropan-2-yl]oxy}phenyl)selane

Guidance literature:: (R)-2-[(1-methoxypropan-2-yl)oxy]phenyl diselenide; With bromine; In tetrachloromethane; dichloromethane; at -78 ℃; for 0.333333h; Inert atmosphere;

methanol; With silver trifluoromethanesulfonate; In tetrachloromethane; dichloromethane; at -78 ℃; for 0.5h; Inert atmosphere;

styrene; In tetrachloromethane; dichloromethane; at -78 ℃; for 2h; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201001272

Reference yield:

: 64658-22-6
(R)-2-phenoxypropan-1-ol

: 1264256-13-4
(2-methoxy-2-phenylethyl)(2-{[(R)-1-methoxypropan-2-yl]oxy}phenyl)selane

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / 0 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: bromine / tetrachloromethane; dichloromethane / 0.33 h / -78 °C / Inert atmosphere

3.2: 0.5 h / -78 °C / Inert atmosphere

3.3: 2 h / -78 °C / Inert atmosphere

With n-butyllithium; bromine; sodium hydride; In tetrahydrofuran; tetrachloromethane; hexane; dichloromethane;
DOI:10.1002/ejoc.201001272

Reference yield:

: 1264256-01-0
(R)-1-(1-methoxypropan-2-yloxy)benzene

: 1264256-13-4
(2-methoxy-2-phenylethyl)(2-{[(R)-1-methoxypropan-2-yl]oxy}phenyl)selane

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: bromine / tetrachloromethane; dichloromethane / 0.33 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

2.3: 2 h / -78 °C / Inert atmosphere

With n-butyllithium; bromine; In tetrahydrofuran; tetrachloromethane; hexane; dichloromethane;
DOI:10.1002/ejoc.201001272