benzyl 1H-pyrrolo[3,2-c]pyridine-1-carboxylate-5-oxide

Base Information

Chemical Name:benzyl 1H-pyrrolo[3,2-c]pyridine-1-carboxylate-5-oxide
CAS No.:1415124-80-9
Molecular Formula:C₁₅H₁₂N₂O₃
Molecular Weight:268.272
Hs Code.:

Synonyms:benzyl 1H-pyrrolo[3,2-c]pyridine-1-carboxylate-5-oxide

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Chemical Property of benzyl 1H-pyrrolo[3,2-c]pyridine-1-carboxylate-5-oxide

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Technology Process of benzyl 1H-pyrrolo[3,2-c]pyridine-1-carboxylate-5-oxide

There total 5 articles about benzyl 1H-pyrrolo[3,2-c]pyridine-1-carboxylate-5-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-99-6
3-Methylpyridine

: 1415124-80-9
benzyl 1H-pyrrolo[3,2-c]pyridine-1-carboxylate-5-oxide

Guidance literature:: Multi-step reaction with 6 steps

1: dihydrogen peroxide / acetic acid / 70 °C / Cooling with ice

2: nitric acid / sulfuric acid / 2 h / 0 - 100 °C

3: dimethyl amine / N,N-dimethyl-formamide / 15 h / 90 °C

4: hydrogen / palladium 10% on activated carbon / methanol / 2 h

5: triethylamine / dichloromethane / 1 h / 0 - 20 °C

6: 3-chloro-benzenecarboperoxoic acid / dichloromethane; Dimethyl ether / 4 h / 20 °C

With hydrogen; dihydrogen peroxide; nitric acid; dimethyl amine; triethylamine; 3-chloro-benzenecarboperoxoic acid; sulfuric acid; palladium 10% on activated carbon; In methanol; Dimethyl ether; dichloromethane; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 1074-98-2
3-methyl-4-nitropyridine N-oxide

: 1415124-80-9
benzyl 1H-pyrrolo[3,2-c]pyridine-1-carboxylate-5-oxide

Guidance literature:: Multi-step reaction with 4 steps

1: dimethyl amine / N,N-dimethyl-formamide / 15 h / 90 °C

2: hydrogen / palladium 10% on activated carbon / methanol / 2 h

3: triethylamine / dichloromethane / 1 h / 0 - 20 °C

4: 3-chloro-benzenecarboperoxoic acid / dichloromethane; Dimethyl ether / 4 h / 20 °C

With hydrogen; dimethyl amine; triethylamine; 3-chloro-benzenecarboperoxoic acid; palladium 10% on activated carbon; In methanol; Dimethyl ether; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1003-73-2
3-picoline-N-oxide

: 1415124-80-9
benzyl 1H-pyrrolo[3,2-c]pyridine-1-carboxylate-5-oxide

Guidance literature:: Multi-step reaction with 5 steps

1: nitric acid / sulfuric acid / 2 h / 0 - 100 °C

2: dimethyl amine / N,N-dimethyl-formamide / 15 h / 90 °C

3: hydrogen / palladium 10% on activated carbon / methanol / 2 h

4: triethylamine / dichloromethane / 1 h / 0 - 20 °C

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane; Dimethyl ether / 4 h / 20 °C

With hydrogen; nitric acid; dimethyl amine; triethylamine; 3-chloro-benzenecarboperoxoic acid; sulfuric acid; palladium 10% on activated carbon; In methanol; Dimethyl ether; dichloromethane; N,N-dimethyl-formamide;