3-[3-(4-{2-(2-{3-[4-(2-Amino-ethyl)-2,6-dibromo-phenoxy]-5-bromo-4-hydroxy-phenyl}-ethylcarbamoyl)-2-[(E)-hydroxyimino]-ethyl}-2,6-dibromo-phenoxy)-5-bromo-4-hydroxy-phenyl]-2-[(Z)-hydroxyimino]-propionic acid

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Chemical Name:3-[3-(4-{2-(2-{3-[4-(2-Amino-ethyl)-2,6-dibromo-phenoxy]-5-bromo-4-hydroxy-phenyl}-ethylcarbamoyl)-2-[(E)-hydroxyimino]-ethyl}-2,6-dibromo-phenoxy)-5-bromo-4-hydroxy-phenyl]-2-[(Z)-hydroxyimino]-propionic acid
CAS No.:210880-85-6
Molecular Formula:C₃₄H₂₈Br₆N₄O₉
Molecular Weight:1116.04
Hs Code.:

3-[3-(4-{2-(2-{3-[4-(2-Amino-ethyl)-2,6-dibromo-phenoxy]-5-bromo-4-hydroxy-phenyl}-ethylcarbamoyl)-2-[(E)-hydroxyimino]-ethyl}-2,6-dibromo-phenoxy)-5-bromo-4-hydroxy-phenyl]-2-[(Z)-hydroxyimino]-propionic acid

Synonyms:3-[3-(4-{2-(2-{3-[4-(2-Amino-ethyl)-2,6-dibromo-phenoxy]-5-bromo-4-hydroxy-phenyl}-ethylcarbamoyl)-2-[(E)-hydroxyimino]-ethyl}-2,6-dibromo-phenoxy)-5-bromo-4-hydroxy-phenyl]-2-[(Z)-hydroxyimino]-propionic acid

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Chemical Property of 3-[3-(4-{2-(2-{3-[4-(2-Amino-ethyl)-2,6-dibromo-phenoxy]-5-bromo-4-hydroxy-phenyl}-ethylcarbamoyl)-2-[(E)-hydroxyimino]-ethyl}-2,6-dibromo-phenoxy)-5-bromo-4-hydroxy-phenyl]-2-[(Z)-hydroxyimino]-propionic acid

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Technology Process of 3-[3-(4-{2-(2-{3-[4-(2-Amino-ethyl)-2,6-dibromo-phenoxy]-5-bromo-4-hydroxy-phenyl}-ethylcarbamoyl)-2-[(E)-hydroxyimino]-ethyl}-2,6-dibromo-phenoxy)-5-bromo-4-hydroxy-phenyl]-2-[(Z)-hydroxyimino]-propionic acid

There total 7 articles about 3-[3-(4-{2-(2-{3-[4-(2-Amino-ethyl)-2,6-dibromo-phenoxy]-5-bromo-4-hydroxy-phenyl}-ethylcarbamoyl)-2-[(E)-hydroxyimino]-ethyl}-2,6-dibromo-phenoxy)-5-bromo-4-hydroxy-phenyl]-2-[(Z)-hydroxyimino]-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 210880-84-5
3-[3-Bromo-5-(2,6-dibromo-4-{2-(2-{3-bromo-5-[2,6-dibromo-4-(2-tert-butoxycarbonylamino-ethyl)-phenoxy]-4-hydroxy-phenyl}-ethylcarbamoyl)-2-[(E)-hydroxyimino]-ethyl}-phenoxy)-4-hydroxy-phenyl]-2-[(Z)-hydroxyimino]-propionic acid

: 210880-85-6
3-[3-(4-{2-(2-{3-[4-(2-Amino-ethyl)-2,6-dibromo-phenoxy]-5-bromo-4-hydroxy-phenyl}-ethylcarbamoyl)-2-[(E)-hydroxyimino]-ethyl}-2,6-dibromo-phenoxy)-5-bromo-4-hydroxy-phenyl]-2-[(Z)-hydroxyimino]-propionic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; 1.) 0 deg C, 5 min, 2.) 24 deg C, 30 min;
DOI:10.1021/jo9721204

Reference yield:

: 58511-69-6
3-(3,5-dibromo-4-hydroxyphenyl)-2-(hydroxyimino)propionic acid

: 210880-85-6
3-[3-(4-{2-(2-{3-[4-(2-Amino-ethyl)-2,6-dibromo-phenoxy]-5-bromo-4-hydroxy-phenyl}-ethylcarbamoyl)-2-[(E)-hydroxyimino]-ethyl}-2,6-dibromo-phenoxy)-5-bromo-4-hydroxy-phenyl]-2-[(Z)-hydroxyimino]-propionic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 46 percent / H₂O₂, soybean peroxidase / acetonitrile; H₂O / 0.17 h / 24 °C

2: 72 percent / 1-hydroxybenzotriazole, DCC / dioxane; dimethylformamide; CH₂Cl₂ / 24 h / 24 °C

3: 99 percent / NaOH, NaHSO₃ / acetonitrile; H₂O / 0.17 h / 24 °C / pH 8.0

4: 95 percent / TFA / CH₂Cl₂ / 1.) 0 deg C, 5 min, 2.) 24 deg C, 30 min

With sodium hydroxide; dihydrogen peroxide; benzotriazol-1-ol; sodium hydrogensulfite; dicyclohexyl-carbodiimide; trifluoroacetic acid; soybean peroxidase; In 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo9721204

Reference yield:

: 210880-88-9
N-(tert-butoxycarbonyl)-3,5-dibromo-4-hydroxy-β-phenethylamine

: 210880-85-6
3-[3-(4-{2-(2-{3-[4-(2-Amino-ethyl)-2,6-dibromo-phenoxy]-5-bromo-4-hydroxy-phenyl}-ethylcarbamoyl)-2-[(E)-hydroxyimino]-ethyl}-2,6-dibromo-phenoxy)-5-bromo-4-hydroxy-phenyl]-2-[(Z)-hydroxyimino]-propionic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 53 percent / H₂O₂, soybean peroxidase / acetonitrile / 0.33 h / 24 °C / pH 5.0

2: 98 percent / CrCl₂ / methanol; CH₂Cl₂ / 0.5 h / 24 °C

3: 72 percent / 1-hydroxybenzotriazole, DCC / dioxane; dimethylformamide; CH₂Cl₂ / 24 h / 24 °C

4: 99 percent / NaOH, NaHSO₃ / acetonitrile; H₂O / 0.17 h / 24 °C / pH 8.0

5: 95 percent / TFA / CH₂Cl₂ / 1.) 0 deg C, 5 min, 2.) 24 deg C, 30 min

With chromium dichloride; sodium hydroxide; dihydrogen peroxide; benzotriazol-1-ol; sodium hydrogensulfite; dicyclohexyl-carbodiimide; trifluoroacetic acid; soybean peroxidase; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo9721204