1-[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]-3-pyridin-4-ylurea

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Chemical Name:1-[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]-3-pyridin-4-ylurea
CAS No.:1197159-90-2
Molecular Formula:C₂₃H₂₆N₈O₃
Molecular Weight:462.511
Hs Code.:

Synonyms:1-[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]-3-pyridin-4-ylurea

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Chemical Property of 1-[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]-3-pyridin-4-ylurea

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Technology Process of 1-[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]-3-pyridin-4-ylurea

There total 2 articles about 1-[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]-3-pyridin-4-ylurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 504-24-5
4-aminopyridine

: 32315-10-9
bis(trichloromethyl) carbonate

: 1197159-91-3
4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)aniline

: 1197159-90-2
1-[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]-3-pyridin-4-ylurea

Guidance literature:: bis(trichloromethyl) carbonate; 4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)aniline; With triethylamine; In dichloromethane; at 0 ℃; for 0.333333h;

4-aminopyridine; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 7597-22-0
2-chloro-4,6-di-morpholin-4-yl-[1,3,5]triazine

: 1197159-90-2
1-[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]-3-pyridin-4-ylurea

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane / 24 h / Reflux

2.1: triethylamine / dichloromethane / 0.33 h / 0 °C

2.2: 2 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; triethylamine; In 1,2-dimethoxyethane; dichloromethane; 1.1: |Suzuki Coupling;