3,5-bis(trifluoromethyl)phenylboronic acid pyrocatechol ester

Base Information

Chemical Name:3,5-bis(trifluoromethyl)phenylboronic acid pyrocatechol ester
CAS No.:73852-85-4
Molecular Formula:C₁₄H₇BF₆O₂
Molecular Weight:332.01
Hs Code.:

Synonyms:3,5-bis(trifluoromethyl)phenylboronic acid pyrocatechol ester

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Chemical Property of 3,5-bis(trifluoromethyl)phenylboronic acid pyrocatechol ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of 3,5-bis(trifluoromethyl)phenylboronic acid pyrocatechol ester

There total 4 articles about 3,5-bis(trifluoromethyl)phenylboronic acid pyrocatechol ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 13292-87-0
dimethylsulfide borane complex

: 328-70-1
3,6-bis(trifluoromethyl)bromobenzene

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 73852-85-4
3,5-bis(trifluoromethyl)phenylboronic acid pyrocatechol ester

Guidance literature:: 3,6-bis(trifluoromethyl)bromobenzene; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 0.25h;

dimethylsulfide borane complex; In diethyl ether; hexane; at -78 ℃; for 0.75h;

benzene-1,2-diol; Further stages;
DOI:10.1021/jacs.0c02306

Reference yield: 62.0%

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 73852-19-4
3,5-bis-trifluromethylphenylboronic acid

: 73852-85-4
3,5-bis(trifluoromethyl)phenylboronic acid pyrocatechol ester

Guidance literature:: In toluene; for 1h; Reflux; Inert atmosphere;
DOI:10.1039/b805437a

Reference yield:

: 13826-27-2
2,2'-bis(1,3,2-benzodioxaborole)

: 328-70-1
3,6-bis(trifluoromethyl)bromobenzene

: 73852-85-4
3,5-bis(trifluoromethyl)phenylboronic acid pyrocatechol ester

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In ethanol; at 80 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.10.118