C₅₁H₇₈O₁₂

Base Information

Chemical Name:C₅₁H₇₈O₁₂
CAS No.:1354728-55-4
Molecular Formula:C₅₁H₇₈O₁₂
Molecular Weight:883.173
Hs Code.:

C<sub>51</sub>H<sub>78</sub>O<sub>12</sub>

Synonyms:C₅₁H₇₈O₁₂

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Chemical Property of C₅₁H₇₈O₁₂

Chemical Property:

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Technology Process of C₅₁H₇₈O₁₂

There total 10 articles about C₅₁H₇₈O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1333473-63-4
(4S,6S)-7-[ (2R,4R,6R)-6-{[(4R,5S,6S)-6-allyl-2,2,5-trimethyl-1,3-dioxan-4-yl]methyl}-2-(4-methoxyphenyl)-1,3-dioxan-4-yl]-4-hydroxy-1-{(4S,6R)-6-[ (3S,4S,E)-4-hydroxy-3,5-dimethylhex-1-enyl]-2,2-dimethyl-1,3-dioxan-4-yl}-6-(4-methoxybenzyloxy)heptan-2-one

: 1354728-55-4
C₅₁H₇₈O₁₂

Guidance literature:: With acetic acid; tetramethylammonium triacetoxyborohydride; In acetonitrile; at -30 - -25 ℃; for 48h; optical yield given as %de; diastereoselective reaction;
DOI:10.1021/jo2012658

Reference yield:

: 1333473-61-2
(4S,5S,6R)-4-allyl-6-{[(2R,4R,6R)-2-(4-methoxyphenyl)-6-{[(2S,4S)-2-(4-methoxyphenyl)-1,3-dioxan-4-yl]methyl}-1,3-dioxan-4-yl]methyl}-2,2,5-trimethyl-1,3-dioxane

: 1354728-55-4
C₅₁H₇₈O₁₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride / dichloromethane / 4.25 h / 0 - 20 °C

1.2: 2 h / Saturated solution

2.1: potassium carbonate; Dess-Martin periodane / dichloromethane / 15 h / 0 - 20 °C

3.1: dicyclohexylboron chloride; triethylamine / diethyl ether / 0.83 h / -10 °C

3.2: 31.08 h / -78 - -26 °C

4.1: acetic acid; tetramethylammonium triacetoxyborohydride / acetonitrile / 48 h / -30 - -25 °C

With dicyclohexylboron chloride; diisobutylaluminium hydride; potassium carbonate; Dess-Martin periodane; acetic acid; triethylamine; tetramethylammonium triacetoxyborohydride; In diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/jo2012658

Reference yield:

: 1333473-70-3
C₅₉H₇₇NO₁₁SSi

: 1354728-55-4
C₅₁H₇₈O₁₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: isopropylmagnesium chloride / tetrahydrofuran; diethyl ether / 2.33 h / -20 - 5 °C

1.2: 0 °C / Saturated solution

2.1: tetrahydrofuran; diethyl ether / 0.53 h / 0 °C

3.1: sodium tetrahydroborate / methanol / 15 h / -50 °C

3.2: Saturated solution

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C

5.1: pyridinium p-toluenesulfonate / dichloromethane / 3 h / 20 °C

6.1: diisobutylaluminium hydride / dichloromethane / 4.25 h / 0 - 20 °C

6.2: 2 h / Saturated solution

7.1: potassium carbonate; Dess-Martin periodane / dichloromethane / 15 h / 0 - 20 °C

8.1: dicyclohexylboron chloride; triethylamine / diethyl ether / 0.83 h / -10 °C

8.2: 31.08 h / -78 - -26 °C

9.1: acetic acid; tetramethylammonium triacetoxyborohydride / acetonitrile / 48 h / -30 - -25 °C

With sodium tetrahydroborate; dicyclohexylboron chloride; tetrabutyl ammonium fluoride; isopropylmagnesium chloride; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; potassium carbonate; Dess-Martin periodane; acetic acid; triethylamine; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/jo2012658