Technology Process of 1-(2-ethyl-4,5-dimethoxyphenyl)-1-ethanone
There total 6 articles about 1-(2-ethyl-4,5-dimethoxyphenyl)-1-ethanone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
trifluorormethanesulfonic acid; titanium(IV) chloride tris(trifluoromethanesulfonate);
DOI:10.1246/bcsj.73.747
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 98 percent / triethylsilane / trifluoroacetic acid / 12 h / 20 °C
2: 66 percent / titanium(IV) chloride tris(trifluoromethanesulfonate); trifluoromethanesulfonic acid
With
triethylsilane;
trifluorormethanesulfonic acid; titanium(IV) chloride tris(trifluoromethanesulfonate);
In
trifluoroacetic acid;
1: Reduction / 2: Acetylation;
DOI:10.1246/bcsj.73.747
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 82 percent / titanium(IV) chloride tris(trifluoromethanesulfonate); trifluoromethanesulfonic acid
2: 98 percent / triethylsilane / trifluoroacetic acid / 12 h / 20 °C
3: 66 percent / titanium(IV) chloride tris(trifluoromethanesulfonate); trifluoromethanesulfonic acid
With
triethylsilane;
trifluorormethanesulfonic acid; titanium(IV) chloride tris(trifluoromethanesulfonate);
In
trifluoroacetic acid;
1: Acetylation / 2: Reduction / 3: Acetylation;
DOI:10.1246/bcsj.73.747
