2-(2-chlorophenyl)-2,3-dihydro-1H-naphtho [1,8-de] [1,3,2]diazaborinine

Base Information

Chemical Name:2-(2-chlorophenyl)-2,3-dihydro-1H-naphtho [1,8-de] [1,3,2]diazaborinine
CAS No.:1338697-46-3
Molecular Formula:C₁₆H₁₂BClN₂
Molecular Weight:278.549
Hs Code.:

Synonyms:2-(2-chlorophenyl)-2,3-dihydro-1H-naphtho [1,8-de] [1,3,2]diazaborinine

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Chemical Property of 2-(2-chlorophenyl)-2,3-dihydro-1H-naphtho [1,8-de] [1,3,2]diazaborinine

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Technology Process of 2-(2-chlorophenyl)-2,3-dihydro-1H-naphtho [1,8-de] [1,3,2]diazaborinine

There total 2 articles about 2-(2-chlorophenyl)-2,3-dihydro-1H-naphtho [1,8-de] [1,3,2]diazaborinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 3900-89-8
2-Chlorobenzeneboronic acid

: 479-27-6
naphthalene-1,8-diamine

: 1338697-46-3
2-(2-chlorophenyl)-2,3-dihydro-1H-naphtho [1,8-de] [1,3,2]diazaborinine

Guidance literature:: In water; at 100 ℃; for 12h; Green chemistry;
DOI:10.1016/j.tet.2021.132205

Reference yield: 57.0%

: 694-80-4
2-bromo-1-chlorobenzene

: 5656-71-3
2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine

: 1338697-46-3
2-(2-chlorophenyl)-2,3-dihydro-1H-naphtho [1,8-de] [1,3,2]diazaborinine

Guidance literature:: 2-bromo-1-chlorobenzene; With iodine; magnesium; In tetrahydrofuran; at 20 ℃; for 1h; Schlenk technique; Inert atmosphere;

2,3-dihydro-1H-naphtho[1,8-de][1,3,2]diazaborinine; In tetrahydrofuran; at 20 ℃; for 3h; Schlenk technique; Inert atmosphere;
DOI:10.1039/d0cc02560g

Reference yield: 86.0%

: 1338697-46-3
2-(2-chlorophenyl)-2,3-dihydro-1H-naphtho [1,8-de] [1,3,2]diazaborinine

: 73183-34-3
bis(pinacol)diborane

: 950511-18-9
1-(2,3-dihydro-1H-naphtho[1,8-de]-1,3,2-diazaborinyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzene

Guidance literature:: With tris(trimethylphosphine)nickel(II) chloride; (2,2,2-trifluoroethoxy)trimethylsilane; cesium fluoride; In tetrahydrofuran; at 120 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol202267t