2-(8-Benzyloxy-3-biphenyl-2-ylmethyl-2-methoxy-indolizin-1-yl)-2-oxo-acetamide

Base Information

Chemical Name:2-(8-Benzyloxy-3-biphenyl-2-ylmethyl-2-methoxy-indolizin-1-yl)-2-oxo-acetamide
CAS No.:182116-34-3
Molecular Formula:C₃₁H₂₆N₂O₄
Molecular Weight:490.558
Hs Code.:

Synonyms:2-(8-Benzyloxy-3-biphenyl-2-ylmethyl-2-methoxy-indolizin-1-yl)-2-oxo-acetamide

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Chemical Property of 2-(8-Benzyloxy-3-biphenyl-2-ylmethyl-2-methoxy-indolizin-1-yl)-2-oxo-acetamide

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Technology Process of 2-(8-Benzyloxy-3-biphenyl-2-ylmethyl-2-methoxy-indolizin-1-yl)-2-oxo-acetamide

There total 12 articles about 2-(8-Benzyloxy-3-biphenyl-2-ylmethyl-2-methoxy-indolizin-1-yl)-2-oxo-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 79-37-8
oxalyl dichloride

: 1026553-31-0
8-Benzyloxy-3-biphenyl-2-ylmethyl-2-methoxy-indolizine

: 182116-34-3
2-(8-Benzyloxy-3-biphenyl-2-ylmethyl-2-methoxy-indolizin-1-yl)-2-oxo-acetamide

Guidance literature:: oxalyl dichloride; 8-Benzyloxy-3-biphenyl-2-ylmethyl-2-methoxy-indolizine; In tetrahydrofuran; at 0 - 20 ℃; for 2h;

With hydroxylamine; In tetrahydrofuran; water; at 0 ℃;

Reference yield:

: 1027544-62-2
(8-Benzyloxy-3-biphenyl-2-ylmethyl-2-methoxy-indolizin-1-yl)-oxo-acetyl chloride

: 182116-34-3
2-(8-Benzyloxy-3-biphenyl-2-ylmethyl-2-methoxy-indolizin-1-yl)-2-oxo-acetamide

Guidance literature:: With ammonium hydroxide; In tetrahydrofuran; for 1h; Ambient temperature;
DOI:10.1021/jm960395q

Reference yield:

: 211299-41-1
o-(iodomethyl)biphenyl

: 182116-34-3
2-(8-Benzyloxy-3-biphenyl-2-ylmethyl-2-methoxy-indolizin-1-yl)-2-oxo-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 2 h / Ambient temperature

2: tetrahydrofuran / 1 h / 0 °C

3: aq. NH₄OH / tetrahydrofuran / 1 h / Ambient temperature

With ammonium hydroxide; In tetrahydrofuran; benzene;
DOI:10.1021/jm960395q