benzyl (+/-)-5-(2-methyl-1,3-dioxolan-2-yl)-2-<((trifluoromethyl)sulfonyl)oxy>pentanoate

Base Information

Chemical Name:benzyl (+/-)-5-(2-methyl-1,3-dioxolan-2-yl)-2-<((trifluoromethyl)sulfonyl)oxy>pentanoate
CAS No.:96929-76-9
Molecular Formula:C₁₇H₂₁F₃O₇S
Molecular Weight:426.411
Hs Code.:

Synonyms:benzyl (+/-)-5-(2-methyl-1,3-dioxolan-2-yl)-2-<((trifluoromethyl)sulfonyl)oxy>pentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (+/-)-5-(2-methyl-1,3-dioxolan-2-yl)-2-<((trifluoromethyl)sulfonyl)oxy>pentanoate

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Technology Process of benzyl (+/-)-5-(2-methyl-1,3-dioxolan-2-yl)-2-<((trifluoromethyl)sulfonyl)oxy>pentanoate

There total 4 articles about benzyl (+/-)-5-(2-methyl-1,3-dioxolan-2-yl)-2-<((trifluoromethyl)sulfonyl)oxy>pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24400-75-7
ethylene-cetal de la bromo-5 pentanone-2

: 96929-76-9
benzyl (+/-)-5-(2-methyl-1,3-dioxolan-2-yl)-2-<((trifluoromethyl)sulfonyl)oxy>pentanoate

Guidance literature:: Multi-step reaction with 3 steps

2: Et₃N, H₂ / 5percent Pt/C / ethyl acetate / 0.27 h / 2585.7 Torr

3: 2,6-di-tert-butyl-4-methylpyridine / CH₂Cl₂ / 1) 0 deg C, 30 min, 2) r.t., 1 h

With 2,6-di-tert-butyl-4-methylpyridine; hydrogen; triethylamine; platinum on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/ja00328a040

Reference yield:

: 7579-36-4
dibenzyl oxalate

: 96929-76-9
benzyl (+/-)-5-(2-methyl-1,3-dioxolan-2-yl)-2-<((trifluoromethyl)sulfonyl)oxy>pentanoate

Guidance literature:: Multi-step reaction with 3 steps

2: Et₃N, H₂ / 5percent Pt/C / ethyl acetate / 0.27 h / 2585.7 Torr

3: 2,6-di-tert-butyl-4-methylpyridine / CH₂Cl₂ / 1) 0 deg C, 30 min, 2) r.t., 1 h

With 2,6-di-tert-butyl-4-methylpyridine; hydrogen; triethylamine; platinum on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/ja00328a040

Reference yield:

: 90741-55-2
benzyl-5-(2-methyl-1,3-dioxolan-2-yl)-2-oxopentanoate

: 96929-76-9
benzyl (+/-)-5-(2-methyl-1,3-dioxolan-2-yl)-2-<((trifluoromethyl)sulfonyl)oxy>pentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N, H₂ / 5percent Pt/C / ethyl acetate / 0.27 h / 2585.7 Torr

2: 2,6-di-tert-butyl-4-methylpyridine / CH₂Cl₂ / 1) 0 deg C, 30 min, 2) r.t., 1 h

With 2,6-di-tert-butyl-4-methylpyridine; hydrogen; triethylamine; platinum on activated charcoal; In dichloromethane; ethyl acetate;
DOI:10.1021/ja00328a040