O-(5'-O-(dimethoxytrityl)thymidin-3'-yl) S-(2,4-dichlorobenzyl) N,N-dimethyl thiophosphoramidite

Base Information

Chemical Name:O-(5'-O-(dimethoxytrityl)thymidin-3'-yl) S-(2,4-dichlorobenzyl) N,N-dimethyl thiophosphoramidite
CAS No.:119619-08-8
Molecular Formula:C₄₀H₄₂Cl₂N₃O₇PS
Molecular Weight:810.735
Hs Code.:

Synonyms:O-(5'-O-(dimethoxytrityl)thymidin-3'-yl) S-(2,4-dichlorobenzyl) N,N-dimethyl thiophosphoramidite

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Chemical Property of O-(5'-O-(dimethoxytrityl)thymidin-3'-yl) S-(2,4-dichlorobenzyl) N,N-dimethyl thiophosphoramidite

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Technology Process of O-(5'-O-(dimethoxytrityl)thymidin-3'-yl) S-(2,4-dichlorobenzyl) N,N-dimethyl thiophosphoramidite

There total 2 articles about O-(5'-O-(dimethoxytrityl)thymidin-3'-yl) S-(2,4-dichlorobenzyl) N,N-dimethyl thiophosphoramidite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40615-39-2
5'-O-(4-4'-dimethoxytrityl)thymidine

: 119619-08-8
O-(5'-O-(dimethoxytrityl)thymidin-3'-yl) S-(2,4-dichlorobenzyl) N,N-dimethyl thiophosphoramidite

Guidance literature:: Multi-step reaction with 2 steps

1: Et(i-Pr)2N / CHCl₃ / 0.17 h / Ambient temperature

2: CHCl₃ / 0.5 h / Ambient temperature

With N-ethyl-N,N-diisopropylamine; In chloroform;

Reference yield:

: 59293-67-3
2,4-dichlorobenzyl mercaptan

: 208458-78-0
bis(dimethylamino)-[5'-(4,4'-dimethoxy)trityl-thymid-3'-yl]phosphorodiamidite

: 119619-08-8
O-(5'-O-(dimethoxytrityl)thymidin-3'-yl) S-(2,4-dichlorobenzyl) N,N-dimethyl thiophosphoramidite

Guidance literature:: In acetonitrile;
DOI:10.1021/ja00188a066

Reference yield:

: 119619-08-8
O-(5'-O-(dimethoxytrityl)thymidin-3'-yl) S-(2,4-dichlorobenzyl) N,N-dimethyl thiophosphoramidite

: 118149-27-2
O-[5'-O-(4,4'-dimethoxytrityl)thymidin-3'-yl] S-(2,4-dichlorobenzyl) O-(3'-O-acetylthymidin-5'-yl) phosphorodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrazole / 0.05 h

2: S₈ / CS₂; pyridine

With 1H-tetrazole; sulfur; In pyridine; carbon disulfide;