N⁴-{3-[(3-Amino-1,3-dimethyl-butylamino)-methyl]-benzyl}-2-methyl-pentane-2,4-diamine

Base Information

• Chemical Name: N⁴-{3-[(3-Amino-1,3-dimethyl-butylamino)-methyl]-benzyl}-2-methyl-pentane-2,4-diamine
• CAS No.: 75813-07-9
• Molecular Formula: C₂₀H₃₈N₄
• Molecular Weight: 334.549

Synonyms:N⁴-{3-[(3-Amino-1,3-dimethyl-butylamino)-methyl]-benzyl}-2-methyl-pentane-2,4-diamine

Chemical Property of N⁴-{3-[(3-Amino-1,3-dimethyl-butylamino)-methyl]-benzyl}-2-methyl-pentane-2,4-diamine

Chemical Property:

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Technology Process of N⁴-{3-[(3-Amino-1,3-dimethyl-butylamino)-methyl]-benzyl}-2-methyl-pentane-2,4-diamine

There total 2 articles about N⁴-{3-[(3-Amino-1,3-dimethyl-butylamino)-methyl]-benzyl}-2-methyl-pentane-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.8%

1,3-di(aminomethyl)benzene (1477-55-0) + 4-amino-4-methylpentan-2-one (625-04-7) → N4-{3-[(3-Amino-1,3-dimethyl-butylamino)-methyl]-benzyl}-2-methyl-pentane-2,4-diamine (75813-07-9)

Guidance literature:

With aluminium; mercury dichloride; In water; 1.) overnight room temp., 2.) 1 h, 90 deg C;

DOI:10.1021/jo00315a020

Reference yield:

4-methyl-pent-3-en-2-one (141-79-7) → N4-{3-[(3-Amino-1,3-dimethyl-butylamino)-methyl]-benzyl}-2-methyl-pentane-2,4-diamine (75813-07-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 27.4 percent / ammonium hydroxide / 4 h / 45 - 50 °C

2: 20.8 percent / mercuric chloride, aluminum / H₂O / 1.) overnight room temp., 2.) 1 h, 90 deg C

With ammonium hydroxide; aluminium; mercury dichloride; In water;

DOI:10.1021/jo00315a020

Reference yield: 12.2%

chloroform (67-66-3,8013-54-5) + N4-{3-[(3-Amino-1,3-dimethyl-butylamino)-methyl]-benzyl}-2-methyl-pentane-2,4-diamine (75813-07-9) + acetone (67-64-1) → C28H46N4O2 (75813-16-0)

Guidance literature:

With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In water; at 0 - 17 ℃;

DOI:10.1021/jo00315a020

upstream raw materials:

1,3-di(aminomethyl)benzene

4-amino-4-methylpentan-2-one

4-methyl-pent-3-en-2-one

Downstream raw materials:

C₂₈H₄₆N₄O₂

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