Technology Process of C32H40N4O6S
There total 6 articles about C32H40N4O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
dichloromethane; isopropyl alcohol;
at 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: water; lithium hydroxide / tetrahydrofuran; methanol / 20 °C
2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran
3: caesium carbonate; thiophenol / N,N-dimethyl-formamide / 20 °C
4: sulfonamide / 1,2-dioxacyclohexane / 100 °C
5: trifluoroacetic acid / dichloromethane
With
sulfonamide; water; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; thiophenol; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hydroxide;
In
tetrahydrofuran; 1,2-dioxacyclohexane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.04.113
- Guidance literature:
-
Multi-step reaction with 6 steps
1: caesium carbonate / N,N-dimethyl-formamide / 60 °C
2: water; lithium hydroxide / tetrahydrofuran; methanol / 20 °C
3: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran
4: caesium carbonate; thiophenol / N,N-dimethyl-formamide / 20 °C
5: sulfonamide / 1,2-dioxacyclohexane / 100 °C
6: trifluoroacetic acid / dichloromethane
With
sulfonamide; water; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; thiophenol; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hydroxide;
In
tetrahydrofuran; 1,2-dioxacyclohexane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.04.113