phenyl phenylsulfonyl ketone O-oxide

Base Information

Chemical Name:phenyl phenylsulfonyl ketone O-oxide
CAS No.:186422-70-8
Molecular Formula:C₁₃H₁₀O₄S
Molecular Weight:262.286
Hs Code.:

Synonyms:phenyl phenylsulfonyl ketone O-oxide

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Chemical Property of phenyl phenylsulfonyl ketone O-oxide

Chemical Property:

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Technology Process of phenyl phenylsulfonyl ketone O-oxide

There total 5 articles about phenyl phenylsulfonyl ketone O-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 186422-69-5
phenyl(phenylsulfonyl)carbene

: 186422-70-8
phenyl phenylsulfonyl ketone O-oxide

Guidance literature:: With oxygen; In gaseous matrix; at -232.2 ℃;
DOI:10.1021/ja962949k

Reference yield:

: 61937-46-0
2-phenyl-1-(phenylsulfonyl)-1,2-epoxyethane

: 186422-70-8
phenyl phenylsulfonyl ketone O-oxide

Guidance literature:: Multi-step reaction with 4 steps

1: 26 percent / BF₃*Et₂O / CH₂Cl₂ / 0.17 h / 0 °C

2: 21 percent / HOOC-C₆H₄-SO₂N₃, aq. NH₃ / CH₂Cl₂ / 20 h / Ambient temperature

3: gaseous matrix / -263.2 °C / Irradiation

4: O₂ / gaseous matrix / -232.2 °C

With ammonium hydroxide; HOOC-C₆H₄-SO₂N₃; boron trifluoride diethyl etherate; oxygen; In dichloromethane;
DOI:10.1021/ja962949k

Reference yield:

: 7205-98-3
chloromethyl phenyl sulfone

: 186422-70-8
phenyl phenylsulfonyl ketone O-oxide

Guidance literature:: Multi-step reaction with 5 steps

1: 67 percent / aq. NaOH, benzyltriethylammonium chloride / acetonitrile / 1.5 h / 0 °C

2: 26 percent / BF₃*Et₂O / CH₂Cl₂ / 0.17 h / 0 °C

3: 21 percent / HOOC-C₆H₄-SO₂N₃, aq. NH₃ / CH₂Cl₂ / 20 h / Ambient temperature

4: gaseous matrix / -263.2 °C / Irradiation

5: O₂ / gaseous matrix / -232.2 °C

With ammonium hydroxide; sodium hydroxide; HOOC-C₆H₄-SO₂N₃; boron trifluoride diethyl etherate; N-benzyl-N,N,N-triethylammonium chloride; oxygen; In dichloromethane; acetonitrile;
DOI:10.1021/ja962949k